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ICPMS daily performance check report, May 15, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 15, 2002.

NYC-WTC_000053505–000053628

Folder label: “ICPMS 5/15/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10136 Sample Date/Time: Wednesday, May 15, 2002 11:06:11 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE10136.075 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean. Cone. Mean Cone. RSD Sample Unit Be 9 9.333 37.627 -0.000 -0.00249 406.79 ug/L LI 6 51796.723 2.604 51796.723 ug/L > Se-1 45 452182.369 0.755 452182.369 ug/L Cr 52 9599.496 1.690 0.006 0.27010 3.69 ug/L Cr 53 2828.135 3.851 0.005 2.03193 4.28 ug/L Mn 55 234048.396 1.686 0.514 14.24566 2.41 ug/L Co 59 964.061 6.303 0.002 0.07264 6.83 ug/L Ni 60 1647.166 3.813 0.004 0.66242 3.36 ug/L Cu 63 77633.206 1.155 0.171 14.56183 1.53 ug/L Cu 65 37299.100 2.564 0.082 14.39249 2.98 ug/L Zn 66 75673.784 1.447 0.750 44.87084 0.49 ug/L Zn 67 11894.229 1.064 0.117 39.75617 2.28 ug/L Zn 68 56341.625 1.016 0.558 44.24860 1.37 ug/L > Ge 72 100005.769 1.214 100005.769 ug/L As 75 5791.927 2.462 0.010 0.47193 8.98 ug/L Se 77 1039.914 2.807 0.004 1.92947 6.37 ug/L Se 82 209.681 29.326 0.002 1.09797 26.09 ug/L As-1 75 1161.753 5.176 1039.751 0.45760 5.78 ug/L Kr 83 1997.906 3.312 -103.358 ug/L Ag 107 126.002 8.944 -0.000 -0.03055 2.89 ug/L Cd 111 93.668 9.920 0.000 0.00524 63.01 ug/L Cd 114 229.159 9.928 0.000 0.01094 34.07 ug/L > In 115 1390351.818 1.310 1390351.818 ug/L Sb 121 349.344 3.908 0.000 0.03442 5.70 ug/L Sb 123 259.237 3.473 0.000 0.03279 4.60 ug/L Ba 135 48805.144 0.411 0.025 16.78023 0.83 ug/L Ba 137 85702.672 1.691 0.044 16.81958 1.16 ug/L Ho 165 1993556.974 0.802 0.017 ug/L > Tb 159 1928341.618 0.879 1928341.618 ug/L Hg 201 55.001 12.727 -0.000 -0.00791 60.79 ug/L Hg 202 134.669 5.623 -0.000 -0.00309 82.39 ug/L n 205 678.699 3.598 -0.000 -0.00068 87.59 ug/L Pb 208 11522.313 2.177 0.005 0.20681 1.65 ug/L

QC Calculated Values

Sample ID: AE10136 Report Date/Time: Wednesday, May 15, 200211:08:07 Page 1

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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