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ICPMS daily performance check report, May 15, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 15, 2002.

NYC-WTC_000053505–000053628

Folder label: “ICPMS 5/15/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10133 Sample Date/Time: Wednesday, May 15, 2002 10:56:19 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE10133.072 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 7.000 42.857 -0.000 -0.01037 74.63 ug/L Li 6 55756.700 1.181 55756.700 ug/L > Sc-1 45 452405.375 0.239 452405.375 ug/L Cr 52 8755.636 1.472 0.004 0.18225 8.00 ug/L Cr 53 1839.871 0.979 0.003 1.18229 1.59 ug/L Mn 55 357738.677 1.152 0.787 21.81491 1.30 ug/L Co 59 436.348 4.499 0.001 0.02729 6.13 ug/L Ni 60 949.393 8.850 0.002 0.37429 9.47 ug/L Cu 63 34297.254 0.888 0.075 6.39076 1.09 ug/L Cu 65 16710.513 1.268 0.036 6.39738 1.51 ug/L Zn 66 3470.697 0.288 0.026 1.55328 2.40 ug/L Zn 67 772.374 2.814 0.006 1.97135 4.69 ug/L Zn 68 3077.885 1.767 0.023 1.86374 2.06 ug/L > Ge 72 104796.035 1.591 104796.035 ug/L As 75 6013.120 1.615 0.009 0.44580 5.02 ug/L Se 77 824.286 1.331 0.001 0.56588 7.45 ug/L Se 82 27.164 242.375 0.001 0.27222 103.44 ug/L As-1 75 1239.097 1.964 1117.095 0.49164 2.18 ug/L Kr 83 1975.568 2.409 -125.696 ug/L Ag 107 431.681 9.626 -0.000 -0.00443 83.86 ug/L Cd 111 121.669 8.315 0.000 0.01354 21.90 ug/L Cd 114 274.354 13.612 0.000 0.01635 30.65 ug/L > In 115 1431910.256 1.026 1431910.256 ug/L Sb 121 803.377 5.117 0.001 0.08300 4.46 ug/L Sb 123 597.257 4.044 0.000 0.07985 3.24 ug/L Ba 135 49337.696 1.416 0.025 16.35475 1.58 ug/L Ba 137 86505.535 1.317 0.043 16.36834 0.76 ug/L Ho 165 2057727.853 1.419 0.012 ug/L > Tb 159 2000047.572 1.143 2000047.572 ug/L Hg 201 80.668 15.500 0,000 0.00744 107.30 ug/L Hg 202 167.003 11.090 0.000 0.00470 103.30 ug/L TI 205 736.371 5.311 0.000 0.00033 356.35 ug/L Pb 208 14042.372 1.669 0.006 0.25243 0.92 ug/L

QC Calculated Values

Sample ID: AE10133 Report Date/Time: Wednesday, May 15, 2002 10:58:16 Page 1

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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