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ICPMS daily performance check report, May 15, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 15, 2002.

NYC-WTC_000053505–000053628

Folder label: “ICPMS 5/15/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10132 Sample Date/Time: Wednesday, May 15, 2002 10:53:02 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\rd1\elandata\Dataset\new york city\AE1 0132.071 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean. Cone. Mean Cone. RSD Sample Unit Be 9 12.667 24.119 0.000 0.00534 159.51 ug/L Li 6 53677.895 1.384 53677.895 ug/L > Sc-1 45 443028.064 0.432 443028.064 ug/L Cr 52 9437.658 0.843 0.006 0.27360 3.74 ug/L Cr 53 2558.719 4.441 0.005 1.84577 4.89 ug/L Mn 55 796300.325 2.663 1.794 49.71877 3.04 ug/L Co 59 854.715 - 0.294 0.002 0.06477 0.25 ug/L Ni 60 2166.280 4.525 0.005 0.89540 5.06 ug/L Cu 63 60681.162 1.793 0.136 11.60317 2.16 ug/L Cu 65 29145.274 1.304 0.065 11.46001 0.91 ug/L Zn 66 7367.725 1.063 0.064 3.81452 2.61 ug/L Zn 67 1425.793 0.360 0.012 4.12043 1.87 ug/L Zn 68 6242.872 1.009 0.054 4.30034 2.78 ug/L > Ge 72 103946.008 1.521 103946.008 ug/L As 75 6130.788 3.627 0.011 0.52484 20.38 ug/L Se 77 907.907 4.690 0.002 1.03441 22.72 ug/L Se 82 36.468 103.954 0.001 0.31562 51.23 ug/L As-1 75 1596.156 3.312 1474.154 0.64878 3.59 ug/L Kr 83 2017.577 1.580 -83.686 ug/L Ag 107 571.024 6.487 0.000 0.00859 37.62 ug/L Cd 111 120.669 4.564 0.000 0.01402 11.41 ug/L Cd 114 300.301 8.398 0.000 0.02095 18.41 ug/L In 115 1403842.732 0.909 1403842.732 ug/L Sb 121 1352.448 11.642 0.001 0.14607 11.20 ug/L Sb 123 1026.882 9.337 0.001 0.14397 8.73 ug/L Ba 135 79623.299 0.101 0.040 26.86952 1.82 ug/L Ba 137 138090.378 1.329 0.070 26.59465 0.43 ug/L Ho 165 2004789.307 1.605 0.003 ug/L > Tb 159 1966198.881 1.725 1966198.881 ug/L Hg 201 129.669 12.202 0.000 0.04072 22.07 ug/L Hg 202 291.341 12.458 0.000 0.04175 21.82 ug/L TI 205 818.712 13.842 0.000 0.00330 95.11 ug/L Pb 208 15831.872 2.907 0.007 0.29739 2.42 ug/L

QC Calculated Values

Sample ID: AE10132 Report Date/Time: Wednesday, May 15, 2002 10:54:58 Page 1

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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