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ICPMS daily performance check report, May 15, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 15, 2002.

NYC-WTC_000053505–000053628

Folder label: “ICPMS 5/15/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10131 Sample Date/Time: Wednesday, May 15, 2002 10:48:47 Sample Type: Spike -1 Sample Description: MSD Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE10131.070 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 19091.884 0.348 0.355 50.36477 2.19 ug/L Li 6 53754.026 1.847 53754.026 ug/L Se-1 45 449993.467 0.893 449993.467 ug/L Cr 52 467288.509 0.463 1.023 47.94343 0.46 ug/L Cr 53 55644.352 1.364 0.123 47.63952 1.28 ug/L Mn 55 1079641.025 2.334 2.395 66.38974 1.46 ug/L Co 59 552042.504 1.644 1.226 47.64763 1.21 ug/L Ni 60 118979.766 1.045 0.264 49.34318 1.82 ug/L Cu 63 261756.494 2.028 0.581 49.50600 2.46 ug/L Cu 65 128296.414 1.768 0.285 49.95594 2.34 ug/L Zn 66 94459.915 1.739 0.886 53.03791 2.14 ug/L Zn 67 16361.212 2.321 0.153 51.86725 3.62 ug/L Zn 68 70962.274 0.952 0.665 52.77841 0.94 ug/L Ge 72 105780.352 1.613 105780.352 ug/L As 75 113540.836 0.631 1.025 50.46043 1.30 ug/L Se 77 11541.100 1.760 0.102 55.08941 0.80 ug/L Se 82 12820.394 1.431 0.122 54.35303 2.84 ug/L As-1 75 103645.176 0.090 103523.174 45.56082 0.09 ug/L Kr 83 2030.580 1.566 -70.683 ug/L Ag 107 533285.965 0.718 0.363 44.92992 1.29 ug/L Cd 111 146876.122 0.421 0.100 47.37161 1.21 ug/L Cd 114 345107.606 1.374 0.235 47.97535 1.22 ug/L > In 115 1467973.970 1.018 1467973.970 ug/L Sb 121 480095.352 0.746 0.327 51.31834 0.83 ug/L Sb 123 371558.619 0.482 0.253 51.66326 0.57 ug/L Ba 135 182978.830 1.391 0.090 60.06760 0.58 ug/L Ba 137 318119.168 1.471 0.157 59.60748 1.30 ug/L Ho 165 2058934.499 0.760 0.002 ug/L > Tb 159 2021815.169 0.816 2021815.169 ug/L Hg 201 5772.890 1.124 0.003 3.67349 1.62 ug/L Hg 202 13184.352 0.756 0.006 3.69971 0.49 ug/L TI 205 1698659.186 3.203 0.840 52.31077 2.67 ug/L Pb 208 2040769.874 1.392 1.008 43.96444 0.58 ug/L

QC Calculated Values

Sample ID: AE10131 Report Date/Time: Wednesday, May 15,2002 10:51:37 Page 1

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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