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ICPMS daily performance check report, May 15, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 15, 2002.

NYC-WTC_000053505–000053628

Folder label: “ICPMS 5/15/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: LRB Sample Date/Time: Wednesday, May 15, 2002 10:17:10 Sample Type: Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\LRB.O66 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean. Conc. Mean Cone. RSD Sample Unit Be 9 7.667 30.123 -0.000 -0.01096 50.94 ug/L Li 6 58567.642 0.625 58567.642 ug/L Se-1 45 502447.291 1.182 502447.291 ug/L Cr 52 7611.261 1.424 -0.002 -0.08556 18.16 ug/L Cr 53 504.352 4.400 0.000 0.03015 41.80 ug/L Mn 55 1984.236 2.514 0.001 0.04037 9.64 ug/L Co 59 153.670 6.773 0.000 0.00154 60.66 ug/L Ni 60 54.334 14.762 0.000 0.00370 74.86 ug/L Cu 63 412.347 14.874 0.000 0.02076 53.03 ug/L Cu 65 230.005 8.663 0.000 0.02024 36.79 ug/L Zn 66 793.043 0.631 0.000 0.02283 13.89 ug/L Zn 67 159.670 8.953 0.000 0.05824 76.42 ug/L Zn 68 622.361 4.387 -0.000 -0.00197 1048.63 ug/L > Ge 72 112243.459 0.351 112243.459 ug/L As 75 5501.117 2.040 0.001 0.05733 71.70 ug/L Se 77 773.209 2.252 0.000 0.05917 124.04 ug/L Se 82 -5.861 1622.613 -0.000 -0.03110 1218.97 ug/L As-1 75 126.002 4.200 0.667 0.00029 793.74 ug/L Kr 83 2092.595 3.204 -109.027 ug/L Ag 107 2160.618 19.701 -0.008 -1.01091 3.40 ug/L Cd 111 97.335 15.388 0.000 0.01908 24.47 ug/L Cd 114 214.339 6.408 0.000 0.0 2074 8.81 ug/L > In 115 1534306.270 0.171 1534306.270 ug/L Sb 121 71.001 18.632 -0.000 -0.0 )433 31.51 ug/L Sb 123 52.607 10.693 -0.000 -0.0)364 20.86 ug/L Ba 135 75.668 14.007 -0.000 -0.00448 76.48 ug/L Ba 137 134.336 4.233 -0.000 -0.00022 452.31 ug/L Ho 165 2090212.809 0.910 -0.007 ug/L > Tb 159 2073470.355 0.352 2073470.355 ug/L Hg 201 107.002 11.019 0.000 0.03 029 23.72 ug/L Hg 202 256.340 20.674 0.000 0.03744 38.49 ug/L Tl 205 860.716 2.789 0.000 0.0 027 7.88 ug/L Pb 208 2600.838 4.526 -0.000 -0.00984 23.89 ug/L

QC Calculated Values

Sample ID: LRB Report Date/Time: Wednesday, May 15, 2002 10:20:09 Page 1

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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