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ICPMS daily performance check report, May 14, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: ICV STD2 60 + 5 PPB Sample Date/Time: Tuesday, May 14, 2002 09:23:26 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd 1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york cityCV STD2 60 + 5 PPB.006 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 31520.869 0.901 0.049- 59.19181 1.85 ug/L Se-1 45 648122.402 1.068 648122.402 ug/L Cr 52 831260.656 0.757 1.268 59.29635 0.33 ug/L Cr 53 100138.244 1.491 0.153 60.32932 2.12 ug/L Mn 55 1411488.262 2.811 2.176 60.62335 2.40 ug/L Ni 60 203227.158 2.166 0.313 59.17386 1.71 ug/L Cu 63 437607.506 1.560 0.675 59.68521 1.25 ug/L Cu 65 211107.480 1.544 0.325 60.15431 0.76 ug/L Zn 66 136879.568 1.187 1.003 59.10262 1.47 ug/L Zn 67 24281.294 0.831 0.178 59.67854 1.10 ug/L Zn 68 102719.465 1.136 0.752 59.45797 1.11 ug/L > Ge 72 135438.686 1.889 135438.686 ug/L As 75 171135.914 1.904 1.219 59.44967 1.01 ug/L Se 77 16186.918 1.455 0.113 59.38136 2.52 ug/L Se 82 17930.084 0.880 0.133 58.56003 2.53 ug/L Kr 83 2449.021 1.075 -55.683 ug/L Ag 107 904977.879 0.661 0.512 59.57769 1.09 ug/L > In 115 1767599.421 0.832 1767599.421 ug/L Sb 121 649830.813 1.271 0.368 59.47956 0.54 ug/L Sb 123 501248.340 1.182 0.284 60.34695 0.68 ug/L Ba 135 207076.256 0.117 0.076 59.27792 0.58 ug/L Ba 137 361581.746 0.825 0.133 58.85268 0.81 ug/L > Tb 159 2715602.008 0.514 2715602.008 ug/L Hg 201 8287.525 0.382 0.003 4.87503 0.31 ug/L Hg 202 18911.173 0.908 0.007 4.87311 1.38 ug/L T1 205 2513191.401 0.556 0.925 61.51808 1.06 ug/L Pb 208 2991825.887 0.426 1.101 58.99372 0.90 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > So-1 45 91.971 Cr 52 Cr 53 Mn 55

Sample ID: ICV STD2 60 + 5 PPB Report Date/Time: Tuesday, May 14, 2002 09:25:39 Page 1

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