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ICPMS daily performance check report, May 9, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 9, 2002.

NYC-WTC_000053212–000053335

Folder label: “ICPMS 5/9/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09677 Sample Date/Time: Thursday, May 09, 2002 13:29:12 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york cit\AE09677.867 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit ’ Be 9 11.667 17.843 0.000- 0.00110 543.63 ug/L > Li 6 57128.026 3.972 57128.026 mg/L > Sc-1 45 470852.170 2.773 470852.170 ug/L Cr 52 8712.594 1.087 0.004 0.18217 8.08 ug/L Cr 53 1519.142 1.045 0.002 0.57657 5.57 ug/L Mn 55 283210.375 2.533 0.595 16.19997 1.08 ug/L Ni 60 946.392 2.676 0.002 0.33194 5.27 ug/L Cu 63 9099.643 0.774 0.019 1.46134 2.10 ug/L Cu 65 4459.138 0.919 0.009 1.43752 3.80 ug/L ' Zn 66 3686.451 3.188 0.005 0.31038 29.59 ug/L Zn 67 823.379 3.583 0.002 0.85097 15.13 ug/L Zn 68 3307.968 0.459 0.008 0.62271 5.87 ug/L > Ge 72 119363.249 2.091 119363.249 ug/L As 75 11294.513 1.534 0.010 0.45797 18.82 ug/L Se 77 1443.755 1.612 0.001 0.42336 13.84 ug/L Se 82 -46.661 111.991 0.000 0.10059 189.06 ug/L As-1 75 963.394 1.194 720.055 0.28238 1.60 ug/L Kr 83 4061.948 0.759 -331.825 ug/L Ag 107 120.669 5.880 -0.000 -0.00290 17.93 ug/L Cd 111 193.337 9.387 . 0.000 0.02859 17.78 ug/L Cd 114 381.778 2.878 0.000 0.02377 5.93 ug/L > In 115 1666354.529 0.258 1666354.529 ug/L Sb 121 549.355 1.823 0.000 0.04439 2.26 ug/L Sb 123 414.403 3.864 0.000 0.04319 4.59 ug/L Ba 135 56964.485 0.453 0.021 15.83276 0.86 ug/L Ba 137 99440.243 0.735 0.037 15.86745 0.14 ug/L Ho 165 2702172.439 0.708 -0.003 ug/L > Tb 159 2659476.618 0.712 2659476.618 ug/L Hg 201 54.334 5.623 -0.000 -0.00336 50.14 ug/L Hg 202 106.668 13.002 -0.000 -0.00299 108.25 ug/L TI 205 687.700 8.827 -0.000 -0.01053 12.87 ug/L Pb 208 8336.237 1.386 0.002 0.10149 2.92 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff

Sample ID: AE09677 Report Date/Time: Thursday, May 09, 2002 13:31:05 Page 1

NYC-WTC_000053309

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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