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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09154 Sample Date/Time: Wednesday, May 08, 2002 11:49:23 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE091 54.791 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 8.667 17.625 -0.000' -0.00540 74.92 ug/L > Se-1 45 467966.583 1.488 467966.583 ug/L Cr 52 8177.759 1.443 0.002 0.07079 33.14 ug/L Cr 53 1493.804 3.925 0.002 0.57854 7.96 ug/L Mn 55 401712.682 1.403 0.845 23.01228 2.95 ug/L Ni 60 1412.457 1.539 0.003 0.48098 1.81 ug/L Cu 63 71077.509 1.104 0.151 11.52487 1.60 ug/L Cu 65 35110.357 0.873 0.075 11.57679 0.99 ug/L Zn 66 90101.225 0.968 0.729 43.90624 0.70 ug/L Zn 67 13781.246 2.177 0.111 37.03537 2.22 ug/L Zn 68 67885.201 0.567 0.549 43.52139 1.22 ug/L Ge 72 122641.629 0.791 122641.629 ug/L As 75 12216.439 2.671 0.010 0.46849 19.41 ug/L Se 77 1508.274 2.289 0.000 0.21829 47.81 ug/L Se 82 -157.285 84.838 -0.001 -0.35101 138.23 ug/L Kr 83 4319.403 2.199 -142.070 ug/L Ag 107 85.335 9.472 -0.000 -0.02059 2.67 ug/L In 115 1793142.997 0.462 1793142.997 ug/L Sb 121 703.368 4.910 0.000 0.04775 5.78 ug/L Sb 123 553.702 1.265 0.000 0.04832 1.15 ug/L Ba 135 65502.799 0.768 0.025 16.98861 0.60 ug/L Ba 137 114934.902 1.490 0.044 17.02279 1.37 ug/L > Tb 159 2625896.569 0.216 2625896.569 ug/L Hg 201 86.668 5.692 -0.000 -0.01969 14.32 ug/L Hg 202 181.670 5.623 -0.000 -0.01957 13.11 ug/L TI 205 1162.753 7.863 -0.000 -0.01085 20.68 ug/L Pb 208 14774.835 1.206 0.005 0.22276 1.53 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rel. % Diff Be 9 > Sc-1 45 91.514 Cr 52 Cr 53 Mn 55

Sample ID: AE09154 Report Date/Time: Wednesday, May 08, 2002 11:51:03 Page 1

NYC-WTC_000053125

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NYC-WTC_000053125Source: NYC Law Department, mirrored locally

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