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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09574 Sample Date/Time: Wednesday, May 08, 2002 15:11:55 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE09574.829 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 14.333 35.802 0.000- 0.01286 114.25 ug/L > Se-1 45 433108.332 1.490 433108.332 ug/L Cr 52 11699.307 1.138 0.011 0.50572 6.42 ug/L Cr 53 2196.954 0.697 0.003 1.29302 3.26 ug/L Mn 55 293914.564 1.854 0.665 18.10935 1.65 ug/L Ni 60 823.712 3.190 0.002 0.29077 5.16 ug/L Cu 63 6067.752 2.312 0.014 1.02841 3.95 ug/L Cu 65 3017.197 0.633 0.007 1.02447 1.69 ug/L Zn 66 1623.828 2.048 0.009 0.52853 4.82 ug/L Zn 67 484.685 9.279 0.003 1.01312 14.42 ug/L Zn 68 1774.858 1.563 0.011 0.87847 3.16 ug/L Ge 72 110624.133 0.830 110624.133 ug/L As 75 10627.504 2.835 0.006 0.29747 32.97 ug/L Se 77 1375.788 1.413 0.001 0.29230 22.07 ug/L Se 82 -70.740 158.601 -0.000 -0.06617 683.94 ug/L Kr 83 3724.800 1.223 -736.672 ug/L Ag 107 166.337 9.320 -0.000 -0.01390 8.36 ug/L In 115 1590256.839 0.542 1590256.839 ug/L Sb 121 578.691 3.432 0.000 0.04361 3.63 ug/L Sb 123 458.405 7.369 0.000 0.04438 8.68 ug/L Ba 135 53184.987 0.383 0.021 14.45848 0.53 ug/L Ba 137 92920.775 1.227 0.037 14.42490 0.65 ug/L > Tb 159 2504888.733 0.594 2504888.733 ug/L Hg 201 72.668 3.178 -0.000 -0.02553 5.22 ug/L Hg 202 137.669 11.261 -0.000 -0.02879 13.97 ug/L TI 205 713.369 10.388 -0.000 -0.02117 8.66 ug/L Pb 208 4515.817 2.934 0.001 0.03477 6.98 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 Se-1 45 84.697 Cr 52 Cr 53 Mn 55

Sample ID: AE09574 Report Date/Time: Wednesday, May 08, 2002 15:13:36 Page 1

NYC-WTC_000053199

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