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ICPMS daily performance check report, May 3, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 3, 2002.

NYC-WTC_000052963–000053092

Folder label: “ICPMS 5/3/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: ICV STD1 30 PPB AND 2 PPB Hg Sample Date/Time: Friday, May 03, 2002 10:36:41 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york cityMCV STD1 30 PPB AND 2 PPBHg.719 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 15498.030 3.230 0.028 ' 29.36372 5.30 ug/L > Se-1 45 548552.073 2.172 548552.073 ug/L Cr 52 351451.261 1.640 0.625 30.54778 3.88 ug/L Cr 53 40003.562 1.132 0.072 29.74518 3.29 ug/L Mn 55 564879.902 1.580 1.026 30.67462 3.18 ug/L Ni 60 75770.758 3.206 0.138 29.36916 5.26 ug/L Cu 63 168571.970 0.900 0.307 30.98421 2.93 ug/L Cu 65 83156.537 2.143 0.151 30.24843 4.28 ug/L Zn 66 55186.214 0.256 0.501 29.52144 1.58 ug/L Zn 67 10200.156 1.704 0.092 30.20685 2.59 ug/L Zn 68 40921.005 2.483 0.371 29.32620 2.99 ug/L > Ge 72 107748.609 1.514 107748.609 ug/L As 75 72370.141 2.225 0.595 29.46307 2.34 ug/L Se 77 6930.850 2.023 0.054 29.99312 3.19 ug/L Se 82 10039.308 0.978 0.064 29.99132 0.83 ug/L Ag 107 328693.281 1.043 0.246 31.04235 2.92 ug/L Cd 111 82776.403 1.978 0.062 29.88519 0.26 ug/L Cd 114 192014.746 1.036 0.144 30.24797 3.00 ug/L > in 115 1337040.751 1.964 1337040.751 ug/L Sb 121 273105.195 1.054 0.204 30.44533 1.01 ug/L Sb 123 203913.213 1.908 0.152 29.95335 0.55 ug/L Ba 135 78005.487 2.519 0.042 29.16302 0.86 ug/L Ba 137 133451.413 0.867 0.072 29.50691 1.01 ug/L Ho 165 1786126.526 1.898 0.016 ug/L > Tb 159 1847031.927 1.716 1847031.927 ug/L Hg 201 2637.743 3.603 0.001 2.04745 4.98 ug/L Hg 202 5991.369 3.572 0.003 2.02453 1.99 ug/L Tl 205 765411.242 0.360 0.414 29.78406 1.66 ug/L Pb 208 1087399.401 0.866 0.588 29.93442 1.19 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 Se-1 45 89.500 Cr 52

Sample ID: ICV STD1 30 PPB AND 2 PPB Hg Report Date/Time: Friday, May 03, 2002 10:39:10 Page 1

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