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GCMS reference standard results for sample AE01330, Feb 2002

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Laboratory report documenting reference standard analysis for organic compounds in sample AE01330 conducted on February 19, 2002.

NYC-WTC_000052855–000052859

Folder label: “GCMS X 1/10/02 A 2/19/02

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NYC 9/11 Public Portal Document

" Data File : C:\HPCHEM\l\DATA\FEB1902\REF.D Vial: 4 Acq On : 19 Feb 2002 12:11 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 21 12:05 2002 Quant Results File: GCMS0208.RES

Quant. Method : C:\HPCHEM\1\METHODS\GCMS02 08.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.31 168 45093 2.94 ug/1 # 86 31) 4-Bromophenyl-phenylether 24.39 248 30202 3.05 ug/1 93 32) Hexachlorobenzene 24.83 284 35804 3.09 ug/1 95 33) Phenanthrene 25.80 178 169931 3.60 ug/1 99 34) Anthracene 25.93 178 151585 3.27 ug/1 98 35) Di-n-butylphthalate 27.69 149 249760 3.78 ug/1 # 98 36) Fluoranthene 29.43 202 157028 3.33 ug/1 # 89 39) Pyrene 30.11 202 163436 3.64 ug/1 # 87 40) Butylbenzylphthalate 32.23 149 68255 2.74 ug/1 98 41) Benzo(a)anthracene 33.74 228 110819 3.37 ug/1 98 42) Bis(2-ethylhexyl)phthalate 34.01 149 120490 3.58 ug/1 97 43) Chrysene 33.87 228 122524 3.79 ug/1 100 45) Di-n-Octylphthalate 35.75 149 115169 2.01 ug/1 # 98 46) Benzo(b)fluoranthene 36.86 252 92873 2.88 ug/1 # 95 47) Benzo(k)fluoranthene 36.94 252 115457 3.56 ug/1 # 96 48) Benzo(a)pyrene 37.87 252 76274 2.85 ug/1 # 94 49) Indeno(1,2,3-cd)pyrene 42.28 276 80708 3.31 ug/1 # 95 50) Dibenz(a,h)anthracene 42.35 278 70405 3.78 ug/1 # 92 51) Benzo(g,h,i)perylene 43.54 276 74776 3.80 ug/1 # 91

(#) = qualifier out of range (m) = manual integration REF.D GCMS0208.M Thu Feb 21 12:08:36 2002 Page 2

NYC-WTC_000052858

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NYC-WTC_000052858Source: NYC Law Department, mirrored locally

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