GCMS analysis results for sample AE01043, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB1502\1043.D Vial: 29 Acq On : 16 Feb 2002 8:32 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.91 0.83 ug/1 65662 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Heptanone, 4-methyl- 128 C8H160 006137-11-7 38 3 Tridcane 184 C13H28 000629-50-5 38 4 2,3 -Pentanedione 100 C5H802 000600-14-6 35 Abundance Scan 204 (6.913 min): 1043.D (-) m/z 43.05 . 100.00% 43 57

71 5000

TITTT I 1+ 85 T’BT 100

m/ z I' ■'' I'1' * I'''' I'''' I ’' ' I'''' I " '' I 6.60 —M 6.80 _ 7.00 _ 7.20 57.0,0 85.07% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #63358: 3-Hexanone 43 57

71 411-PT 5000 6.60 6.80 7.00 7.20____ 100 m/ z 71.0,0 54.31% ................ 11’ 185 ■

UL_ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 57 29 43 —r41 ■ 1111* 71 __ 6.60 6.80_ 7.00 7.20 _ 5000 86 m/z 41.05 37.14%

99 128 m/z-> Abundance 20 30 40 43 50 60 57 70 80 i ■ •'' I ■ 11" 1111 " 111" I “i " " r '1' 11'111 90 100 110 120 130 140 150 160 170 180 190 #69019: Tridecane 6.60 6.80 VWW 7.00 7.20 m/z 100.05 27.45% 71 5000 55 27 99 113 127 ... . 0T‘‘uuuumgu, i 184 •■■ ■I • T m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 6.60 6.80 7.00 7.20

1043.D GCMS0208.M Wed Feb 20 14:29:05 2002 Page 1

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