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GCMS analysis report for sample AE01041, Feb 2002

Machine-extracted title · confidence 50%

GC/MS analysis report for sample AE01041 showing surrogate recovery data generated on February 25, 2002.

NYC-WTC_000052799–000052804

Folder label: “GCMS X 1/17/02 A 2/16/02

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. -0 -.02C

Nc9mPuD"Ceporaibocume"" LSC Area Percent Report

.CHEM\ l \ DATA\ FEB1502\1041.D Vial: 30 Data Feb 2002 9:30 pm Operator: 209 Acq On e/ms scan 1/17 Inst : GC/MS Multiplr: 1.00 Sample .ion Params: LSCINT.P MISc MS : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE integrator) —eth : 209 625/TCLP calibration table ting : OFF Filtering: 5 "iing : 1 Min Area: 1 % of largest Pe. art Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 8.213 336 345 351 rBV 13731 31905 1.46% 0.304% 2 12.335 788 794 805 rBV 722440 1679594 76.97% 15.993% 3 15.970 1184 1190 1202 rBV 1007136 2038525 93.42% 19.411% 4 21.286 1763 1769 1785 rBV 1099152 2182039 100.00% 20.778% 5 25.738 2247 2254 2264 rBV 979148 2028499 92.96% 19.316%

6 30.815 2802 2807 2812 rVB 121958 230259 10.55% 2.193% 7 33.798 3126 3132 314} rBV 608521 1344458 61.61% 12.802% 8 38.086 3589 3599 361; rBV2 324419 966608 44.30% 9.204%

Sun of corrected areas: 10501887 1041.D GCMS0208.M Wd Feb 20 14:27:09 2002

..

NYC-WTC_000052804

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NYC-WTC_000052804Source: NYC Law Department, mirrored locally

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