Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
NYC-WTC_000052644–000052652Folder label: “GCMS X 1/15/02 A 2/28/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
‘ Data File : C:\HPCHEM\l\DATA\FEB1402\1046.D Vial: 9 Acq On : 14 Feb 2002 5:49 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 19 12:55 2002 (Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.34 152 263314 20.00 ug/1 0.00 10) Naphthalene-d8 15.99 136 1008261 20.00 ug/1 0.00 17) Acenaphthene-dlO 21.30 164 538823 20.00 ug/1 0.00 29) Phenanthrene-dlO 25.75 188 797239 20.00 ug/1 -0.02 38) Chrysene-dl2 33.82 240 567198 20.00 ug/1 -0.03 44) Perylene-dl2 38.10 264 365764 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.82 235 45937 5.74 ug/mL 0.33 Spiked Amount 5.000 Recovery = 114.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.04 128 196 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.64 163 2439 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.77 149 5053 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 1046.D GCMS0308.M Thu Mar 14 15:25:43 2002 Page 1
NYC-WTC_000052644
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NYC-WTC_000052884
Technical document listing calibration standards and response factors for gas chromatography-mass spectrometry analysis of TCLP samples in February 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052630
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052600
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052707
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052832
GC/MS analysis report for sample AE01043 showing surrogate recovery data generated on February 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052586
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052805
GC/MS analysis report for sample AE01226 showing surrogate recovery data generated on February 25, 2002.
Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052714
Calibration table and instrument data for GC/MS analysis generated on February 12 and 19, 2002.
Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016118
Calibration table for GCMS analysis listing surrogate compounds and response factors from January 16, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009650
Calibration table page listing internal standards and response factors for GCMS analysis.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003803
GCMS analysis report dated March 6, 2002, listing other unknown compounds and surrogate recovery data for a different sample.
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NYC-WTC_000052513
Document page with illegible text or heavy corruption, likely part of the GCMS sample series from January-February 2002.
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NYC-WTC_000052514
Document page with illegible text or heavy corruption, likely part of the GCMS sample series from January-February 2002.
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NYC-WTC_000052517
GCMS analysis report for sample AE01002 listing concentrations of various organic compounds detected in March 2002.
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NYC-WTC_000052525
Quantitative analytical results for sample AE01002 listing concentrations of various organic compounds detected in March 2002.
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NYC-WTC_000052531
GCMS blank analysis report for sample AE01002 showing no detected compounds in March 2002.
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