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GCMS calibration table for TCLP analysis, February 2002

Machine-extracted title · confidence 100%

Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.

NYC-WTC_000052600–000052606

Folder label: “GCMS X 1/15/02 A 2/28/02

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Scanned page image, NYC-WTC_000052603
OCR text

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NYC 9/11 Public Portal Document - —- — *\CDUL L

Data File : C:\HPCHEM\l\DATA\FEB1402\1004.D Vial: 10 . Acq On : 14 Feb 2002 6:47 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.345 789 795 806 rVB 740454 1926930 73.35% 14.465% 2 15.990 1186 1192 1205 rBV 1191865 2417825 92.04% 18.150% 3 21.305 1764 1771 1793 rBV 1309761 2626878 100.00% 19.719% 4 25.748 2249 2255 2266 rBV2 1200842 2536253 96.55% 19.039% 5 27.713 2463 2469 2474 rBV 23557 42149 1.60% 0.316%

6 30.825 2803 2808 2813 rBV 172115 320867 12.21% 2.409% 7 33.818 3127 3134 3151 rBV2 883593 1948734 74.18% 14.629% 8 36.297 3399 3404 3416 rBV 29752 90735 3.45% 0.681% 9 38.105 3592 3601 3621 rBV2 470790 1411017 53.71% 10.592%

Sum of corrected areas: 13321388

1004.D GCMS0308.M Thu Mar 14 15:28:08 2002

NYC-WTC_000052603

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NYC-WTC_000052603Source: NYC Law Department, mirrored locally

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