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GCMS analysis results for sample AE01002, March 2002

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Laboratory report documenting GCMS analysis of sample AE01002 conducted on March 14, 2002.

NYC-WTC_000052578–000052585

Folder label: “GCMS X 1/15/02 A 2/28/02

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NYC 9/11 Public Portal Document

: \MSD< 8 Feb File : C:\MSDCHEM\1\DATA\022802\01002FB.D Vial: 15 ? C MS ; n : 28 Feb 2002 10:26 pm Operator: McLean $ e : GC MS SCAN 2/27 Inst : Instrumen n Par.

tegration Params: BENZO.P : Time: Mar 13 10:56:19 2002 Multiplr: 1.00

Quant Results File: 5080202.RES d lar 13

: C:\) : Qua: Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) : Mon : Quantitation For Method 508gcscan : ini Update : Mon Feb 25 19:17:14 2002 : 508. nse via : Initial Calibration cq Meth : 508SCAN nd rnal Standards R.T. Qlon Response Cone Units Dev(Min) (k) fl 1,4-Dichlorobenzene-d4 9.58 150 965091 20.00 ug/L 0.00 (a) py Naphthalene-d8 13.05 136 2613886 20.00 ug/L 0.00 (1,2, Acenaphthene-diO 18.16 164 1460921 20.00 ug/L 0.00 (a,h) Phenanthrene-dl0 22.52 188 2180698 20.00 ug/L 0.00 (g,h, i Chrysene-dl2 30.33 240 1995351 20.00 ug/L -0.03 Perylene-dl2 34.20 264 1278577 20.00 ug/L -0.02

:m Monitoring Compounds 2,4-ddd surr 27.46 235 184457 5.33 ug/L 0.00 ked Amount 5.000 Recovery = 106.60%

t Compounds Qvalue N-nitroso-dimethyl amine 0.00 74 0 N.D. bis(2-chloroethyl) ether 0.00 93 0 N.D. 1,3 - Dichlorobenze 0.00 146 0 N.D. 1,4 - Dichlorobenzene 0.00 146 0 N.D. 1,2 - Dichlorobenzene 0.00 146 0 N.D. 2,2 ' - oxybis (1-Chloropr 0.00 45 0 N.D. -Nitroso-di-n-propylamine 0.00 70 0 N.D. iexachloroethane 0.00 117 0 N.D. Jitrobenzene 0.00 77 0 N.D. 'sophorone 0.00 82 0 N.D. is(2-Chloroethoxy) methan 0.00 93 0 N.D. .,2,4-Trichlorobenzene 0.00 180 0 N.D. aphthalene 0.00 128 0 N.D. exachlorobutadiene 0.00 225 0 N.D. exachlorocyclopentadiene 0.00 237 0 N.D. -chloronaphthalene 0.00 162 0 N.D. imethylphthalate 0.00 163 0 N.D. ,6-Dinitrotoluene 0.00 165 0 N.D. d cenaphthylene 0.00 152 0 N.D. cenaphthene 0.00 153 0 N.D. ,4-Dinitrotoluene 0.00 165 0 N.D. iethylphthalate 0.00 149 0 N.D. -Chlorophenyl-phenyl ethe 0.00 204 0 N.D. luorene 0.00 166 0 N.D. zobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. •Nitrosodiphenylamine 0.00 169 0 N.D. Bromophenyl-phenyl ether 0.00 248 0 N.D. xachlorobenzene 0.00 284 0 N.D. enanthrene 0.00 178 0 N.D. thracene 0.00 178 0 N.D. -n-butylphthalate 24.67 149 6580 0.05 ug/L 79 uoranthene 0.00 202 0 N.D. rene 0.00 202 0 N.D. tylbenzylphthalate 0.00 149 0 N.D. nzo (a) antracene 0.00 228 0 N.D. d s (2-ethylhexyl) phthala 30.94 149 13650 0.15 ug/L 96 rysene 0.00 228 0 N.D. d -n-Octylphthalate 0.00 149 0 N.D. izo (b) fluoranthene 0.00 252 0 N.D. alifier o D 508020 alifier out of range (m) = manual integration D 5080202.M Wed Mar 13 10:57:09 2002 Page 1

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