NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\1\DATA\022802\0226LB.D Vial: 6
«Acq On : 28 Feb 2002 3:05 pm Operator: McLean
• Sample : GC MS SCAN 2/27 Inst : Instrumen
Mise : Multiplr: 1.00
MS Integration Params: BENZO.P
Quant Time: Mar 13 06:39:56 2002 Quant Results File: 5080202.RES
Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator)
- Title : Quantitation For Method 508gcscan
Last Update : Mon Feb 25 19:17:14 2002
Response via : Initial Calibration
DataAcq Meth : 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 9.58 150 1109289 20.00 ug/L 0.00
10) Naphthalene-d8 13.05 136 2907742 20.00 ug/L 0.00
17) Acenaphthene-diO 18.16 164 1636799 20.00 ug/L 0.00
29) Phenanthrene-diO 22.52 188 2498938 20.00 ug/L 0.00
38) Chrysene-dl2 30.34 240 2345323 20.00 ug/L -0.02
44) Perylene-dl2 34.21 264 1459711 20.00 ug/L 0.00
System Monitoring Compounds
37) 2,4-ddd surr 27.46 235 213713 5.39 ug/L 0.00
Spiked Amount 5.000 Recovery = 107.80%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-chloroethyl) ether 0.00 93 0 N.D.
4) 1,3 - Dichlorobenze 0.00 146 0 N.D.
5) 1,4 - Dichlorobenzene 0.00 146 0 N.D.
6) 1,2 - Dichlorobenzene 0.00 146 0 N.D.
7) 2,2 ’ - oxybis (1-Chloropr 0.00 45 0 N.D.
3) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 ' 0 N.D.
13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 0.00 128 0 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 18.16 165 211255 9.28 ug/L #
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 0.00 149 0 N.D.
26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
30) N-Nitrosodiphenylamine 0.00 169 0 N.D.
31) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D.
32) Hexachlorobenzene 0.00 284 0 N.D.
33) Phenanthrene 0.00 178 0 N.D.
34) Anthracene 0.00 178 0 N.D.
35) Di-n-butylphthalate 0.00 149 0 N.D.
3 6) Fluoranthene 0.00 202 0 N.D.
39) Pyrene 0.00 202 0 N.D.
40) Butylbenzylphthalate 0.00 149 0 N.D.
41) Benzo (a) antracene 0.00 228 0 N.D. d
42) Bis (2-ethylhexyl) phthala 30.94 14.9 25143 0.24 ug/L 93
43) Chrysene 0.00 228 0 N.D. d
45) Di-n-Octylphthalate 0.00 149 0 N.D.
46) Benzo (b) fluoranthene 0.00 252 0 N.D.
(#) = qualifier out of range (m) = manual integration
0226LB.D 5080202.M Wed Mar 13 06:40:54 2002 Page 1
NYC-WTC_000038392
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