Technical data sheet recording GCMS Method 508 calibration results including response factors and percent relative standard deviation for various compounds.
NYC-WTC_000052332–000052354Folder label: “GCMS X 1/14/02 A 2/22 - 2/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)
Data File : C:\MSDCHEM\1\DATA\022102\CAL3.D Vial: 5 Acq On : 21 Feb 2002 6:36 pm Operator: McLean Sample : 2 MIX Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Feb 27 06:06:05 2002 <Quant Results File: 5080202.RES
Quant Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Mon Feb 25 19:17:14 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 9.59 150 1305615 20.00 ug/L 0.00 10) Naphthalene-d8 13.07 136 3111304 20.00 ug/L 0.00 17) Acenaphthene-diO 18.18 164 1640749 20.00 ug/L 0.00 29) Phenanthrene-diO 22.53 188 2648395 20.00 ug/L 0.00 38) Chrysene-dl2 30.37 240 2309596 20.00 ug/L 0.00 44) Perylene-dl2 34.23 264 1685718 20.00 ug/L 0.00
System Monitoring Compounds 37) 2,4-ddd surr 27.47 235 27242 0.65 ug/L 0.00 Spiked Amount 5.000 Recovery = 13.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.58 74 1010396 25.59 ug/L 100 3) bis(2-chloroethyl) ether 9.04 93 1504784 24.34 ug/L 98 4) 1,3 - Dichlorobenze 9.42 146 1452223 24.88 ug/L 99 5) 1,4 - Dichlorobenzene 9.63 146 1440950 24.84 ug/L 99 6) 1,2 - Dichlorobenzene 10.01 146 1331249 24.79 ug/L 100 7) 2,2 ' - oxybis (l-Chloropr 10.48 45 3743397 25.04 ug/L 100 8) N-Nitroso-di-n-propylamine 10.83 70 1226748 25.87 ug/L 99 9) Hexachloroethane 10.89 117 589205 25.13 ug/L 96 11) Nitrobenzene 11.17 77 1815012 25.03 ug/L 97 12) Isophorone 11.88 82 3294188 24.90 ug/L 100 13) bis(2-Chloroethoxy) methan 12.61 93 2008036 25.04 ug/L 99 14) 1,2,4-Trichlorobenzene 12.94 180 1127528 25.48 ug/L 99 15) Naphthalene 13.13 128 4102045 25.07 ug/L 100 16) Hexachlorobutadiene 13.57 225 619421 25.21 ug/L 99 18) Hexachlorocyclopentadiene 15.64 237 441724 27.53 ug/L 96 19) 2-chloronaphthalene 16.55 162 2404425 25.64 ug/L 100 20) Dimethylphthalate 17.65 163 2880377 25.75 ug/L 98 21) 2,6-Dinitrotoluene 17.76 165 598960 26.24 ug/L 96 22) Acenaphthylene 17.73 152 3303807 25.63 ug/L 99 23) Acenaphthene 18.28 153 2267134 25.32 ug/L 99 24) 2,4-Dinitrotoluene 18.91 165 867249 26.47 ug/L 94 25) Diethylphthalate 19.79 149 2523959 26.34 ug/L 100 26) 4-Chlorophenyl-phenyl ethe 19.94 204 1296362 26.02 ug/L 99 27) Fluorene 19.81 166 2583376 25.31 ug/L 98 28) Azobenzen/ 1,2-Diphenylhyd 20.40 77 3738146 25.54 ug/L 96 30) N-Nitrosodiphenylamine 20.33 169 1807922 25.58 ug/L 99 31) 4-Bromophenyl-phenyl ether 21.36 248 717877 25.67 ug/L 95 32) Hexachlorobenzene 21.40 284 728549 25.31 ug/L 95 33) Phenanthrene 22.61 178 3866485 25.18 ug/L 99 34) Anthracene 22.76 178 3718815 25.23 ug/L 100 35) Di-n-butylphthalate 24.69 149 4604540 25.95 ug/L 99 36) Fluoranthene 26.11 202 4479488 25.36 ug/L 100 3 9) Pyrene 26.74 202 4626604 24.65 ug/L 98 40) Butylbenzylphthalate 29.10 149 2115536 26.31 ug/L 96 41) Benzo (a) antracene 30.33 228 3833983 25.30 ug/L 99 42) Bis (2-ethylhexyl) phthala 30.96 149 2791466 26.65 ug/L 97 43) Chrysene 30.44 228 3642789 24.66 ug/L 99 45) Di-n-Octylphthalate 32.80 149 4781048 27.66 ug/L 98 46) Benzo (b) fluoranthene 33.29 252 3521740 24.97 ug/L 99
(#) = qualifier out of range (m) = manual integration CAL3.D 5080202.M Wed Feb 27 06:06:09 2002 Page 1
NYC-WTC_000052340
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Reviewed calibration data sheet for GCMS Method 508 listing retention times and concentrations for deuterated internal standards.
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Reference standard analysis report for volatile organic compounds using GCMS on March 25, 2002.
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