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GCMS analysis results for sample AE00472, Feb 26 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS scan results for sample AE00472, including detection of unknown compounds and surrogate recovery data.

NYC-WTC_000052271–000052290

Folder label: “GCMS X 1/11/02 A 2/7/02

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Scanned page image, NYC-WTC_000052273
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NYC 9/11 Public Portal Document Quantitation Report \IOL RVASws/

. Data File : C:\MSDCHEM\l\5973N\02FEB07\00472A.D Vial: 3 Acq On : 7 Feb 2002 12:42 pm Operator: Sample : 508 scan re-ext. Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Feb 20 15:39:27 2002 Quant Results File: HP020702.RES Quant Method : C:\MSDCHEM\l..-\HP020702.M (RTE Integrator) Title : 508 scan method Last Update : Wed Feb 20 11:48:57 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.71 152 1543502 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 6491977 20.00 ug/L -0.01 17) Acenaphthene-diO 18.34 164 3308595 20.00 ug/L 0.00 29) Phenanthrene-diO 22.63 188 5392932 20.00 ug/L -0.01 38) Chrysene-dl2 30.49 240 4626632 20.00 ug/L -0.03 44) Perylene-dl2 34.42 264 3229802 20.00 ug/L -0.03

System Monitoring Compounds 37) 2,4-DDD 27.73 235 509802 5.74 ug/L 0.00 Spiked Amount 5.000 Recovery = 114.80%

Target Compounds Qvalue 20) Dimethylphthalate 18.34 163 533995 2.66 ug/L # 58 21) 2,6-Dinitrotoluene 18.34 165 416326 8.98 ug/L # 27

(#) = qualifier out of range (m) = manual integration 00472A.D HP020702.M Wed Feb 20 15:39:27 2002 Page 1

NYC-WT C_000052273

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NYC-WTC_000052273Source: NYC Law Department, mirrored locally

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