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GCMS analysis results for sample AE00838, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00838 including surrogate recovery and unknown compounds.

NYC-WTC_000052187–000052204

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052187
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\MSDCHEM\1\5973N\02JAN31\00831.D Vial: 4 Acq On : 31.Jan 2002 1:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 f Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Feb 01 08:46:01 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.71 152 1513969 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 6389561 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 3350546 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 5363324 20.00 ug/L -0.02 38) Chrysene-dl2 30.49 240 4706327 20.00 ug/L -0.02 44) Perylene-dl2 34.42 264 3342876 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 374711 4.42 ug/L 0.00 Spiked Amount 5.000 Recovery = 88.40%

Target Compounds Qvalue 20) Dimethylphthalate 18.34 163 532685 2.41 ug/L # 56 21) 2,6-Dinitrotoluene 18.34 165 421686 9.77 ug/L # 17 42) Bis(2-ethylhexyl)phthalate 31.11 149 68525 0.84 ug/L 91

(#) = qualifier out of range (m) = manual integration 00831.D SCAN508.M Fri Feb 01 15:31:30 2002 Page 1

NYC-WTC_000052187

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NYC-WTC_000052187Source: NYC Law Department, mirrored locally

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