GCMS results for sample AE00700, Feb 13 2002

NYC 9/11 Public Portal Document 2 —ptL ICDUL

Data File : C:\MSDCHEM\l\5973N\02FEB01\00700.D Vial: 7 . Acq On : 1 Feb 2002 7:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 METHOXYAMINE HYDROCHLORIDE Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 3.76 0.06 ug/L 24622 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 METHOXYAMI HYDROCHLORIDE 47 CH5NO 000067-62-9 3 2 Butane, 2 -dimethyl- 86 C6H14 000079-29-8 3 3 Butane, ,3-dimethyl- 86 C6H14 000079-29-8 3 4 Butane, 2,3-dimethyl- (CAS) $$ 2... 86 C6H14 000079-29-8 2 Abundance Scan 34 (3.762 min): 00700.D (-) m/z 43.10 100.00% 43

n/z-> 5000

0b 5 86 TWP "i ■ ■ ■ ■i• • ■ ■ i ■■ ■ ■111' ■ i"" i■ ■ ■ ■ i' ■ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 147,51 । | । । rri ! । | I । . । | I 1‘' ■l m/z A 3.60 1 3.80 44.00 4.00 4.20 9.58% Abundance #318: METHOXYAMINE HYDROCHLORIDE 31 4447

5000 360 3.80 4.00 4.20 m/z 47.00 8.63% 15 Oh "i""r• 111" " i ■ ■ Tr r '" i " " 11"1111" I r " ' r ' " i " " i' " ■ i n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4286: Butane, 2,3-dimethyl- 43 AAAAAMAA 360 3.80 4.00 4.20 5000 m/z 49.00 3.70%

ob 11 " ' i" " i " ■ ■ r ' " i — 39 55 1111 IT 111 > 1111 71

TT i' ■'' i 86 TT Tr AAPMAN m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4284: Butane, 2,3-dimethyl- 43 3.60 3.80 4.00 4.20 m/z 85.90 2.21%

5000

27 71 wwAMWvd m/z-> 0 5 4 4 39

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 55 — 111111 L T 86 TT 3.60 3.80 4.00 4.20

10700.D SCAN508.M Mon Feb 04 08:40:51 2002 Page 5

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