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GCMS analysis results for sample AE00613, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.

NYC-WTC_000051586–000051604

Folder label: “GCMS X 1/9/02 A 1/29/02

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Scanned page image, NYC-WTC_000051592
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN29\00613.D Vial: 2 ■ Acq On : 29 Jan 2002 3:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Butanoic acid, methyl ester... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.

3.61 0.12 ug/L 59435 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 78 2 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 78 3 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 78 4 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 78 Abundance Scan 21 (3.614 min): 00613. D (-) m/z 43.10 100.00% 48 74

5000 59 87 1 TTuutuuTtutTgTT. A 3 50 3.60 3.70 3.80 3.90 4.00 A ■ ■ । । ■ i ......... 1 149 . I.......... 1 ■ ■ t ■ ' ' ■ i ■ • ' ■ i > i • । । । > r ■ ■ T"T m/ z 74.00 80.36% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance ;#9227: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 74

5000 Tt1n‘‘/0——V * ‘ _______ 0tT—UTTT"TCH ""II"IIIT 3.50 3.60 3.70 3.80 3.90 4.00 59 87 m/z 71.10 72.40% - 69 102 i'. ■ i ■ ■ ■ .‘i ' . TTT ‘ 1 I 1 1 1 ' i ■ ' ■ ■ i 1 ' 1 1 I /z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9220: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 mmPmmPP —A 74 3.50 3.60 3.70 3.80 3.90 4.00 15 m/z 41-10 33.73% 5000 27 59 87 33 i11 ■ t 1 >1 ।' t . ; . . 11 .... 1.... 102 ■ 1 i ' 1 1 ' i ' ■ ■ ■ i ' ' ' ■ i ' 1 i ■ ' 1 ' i ' 1 ■ ■ । ' ■ 1 r । m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9222: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... A■1111 43 74 3.50 3.60 3.70 3.80 3.90 4.00 m/z 59.10 31.49%

5000 59 87

33 102 ' ■ i 1 ' ■ ■ i ■ ' 1 ' 1 1 ■ 1 ' I I'1 1 I 1 1 1 1 I 1 ' 1 1 1 1 1 1 I 1 1 ' 1 i ■ ■ ■ ■ i 1 ■ ' 1 i "IT ""I"11 r’"'!' F‘‘IF+II m/z—> 10 20 30 40 50 60 70 80 90 100 110 3 50 3.60 3.70 3.80 3.90 4.00

)0613.D SCAN508.M Wed Jan 30 09:02:08 2002 Page 3

NYC-WTC_000051592

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NYC-WTC_000051592Source: NYC Law Department, mirrored locally

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