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GCMS analysis results for sample AE00555, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00555 conducted on February 1, 2002.

NYC-WTC_000051531–000051548

Folder label: “GCMS X 1/9/02 A 1/29/02

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NYC 9/11 Public Portal Document

DCa11 puil ACDWA

Data File : C: \MSDCHEM\1\5973N\02JAN29\00555.D Vial: 1 ■ Acq On 29 Jan 2002 : 2:32 pm Operator: Sample 508 scan : Inst : Instrumen Mise January 29, 2002 : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 11 1,4-Cyclohexadiene, 6-methy... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 29.68 0.04 ug/L 32331 Chrysene-dl2 30.50 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Cyclohexadiene, 6-methylene-... 244 C19H16 018636-59-4 50 P 2 4-Pyrimidinol , 2-(1-methylethyl)... 244 C14H16N2O2 000000-00-0 50 3 enxo-2-(phenylimino)-3-methyl-1, ... 244 C15H20N2O 105545-43-5 50 A(OA 4 2H-Pyran-2-one, 6-[2-E-(2-hydrox. .. 244 C14H12O4 132405-77-7 9 Abundance Scan 2304 (29.678 min): 00555. D (-) m/z 244.10 100.00% 24.4

5000 122 T-r-p-r 86............... । 29.40 29.60 29.80 30.00 44 ■ 1 i 1 ■ m/z 243.10 38.40% /z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #179623:1,4-Cyclohexadiene, 6-methylene-3,3-diphenyl- $$ ... 244

5000 1 ' i ' 1 i ■ 29.40 29.60 29.80 30.00 167 m/z 121.90 26.14% 229 .. 152 n/z-> ■ ' i ‘ 40 114 |, ‘ i ■ ■ ■ ■ I 1 ■ ■ 1 i ■ 1 ' ' i 1 1 1 1 I 1 1 1 1 I 60 80 100 120 140 160 -215 180 200 220 240 Abundance #179011: 4-Pyrimidinol, 2-(1-methylethyl)-6-[(phenoxy)methyl] 244

29.40 29.60 29.80 30.00 5000 m/z 245.20 15.34% 70 158 87 123 138 — 1 ? 188199 ,.1225.. 21 5225 1 ' i ' ■ ■ 1 i ' ■ ■ ■ i ■ ' ' ■ i ■ ' l । ■ i ■ ■ /z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #179263: enxo-2-(phenylimino)-3-methyl-1,3,2-perhydrobenzo... 1 TTT 24 4 29.40 29.60 29.80 30.00 m/Z 85.90 11.41%

5000 106 ... 119 149 161 44 95 132

m/z-> ' ■ i1 40 60 80 XL 100 120 140 160 175 180 200 ' I ' ' 1 1 i ' ' ' ' I 200 220 240 — ' ' 1 1 ’ 29.40 29.60 29.80 30.00 IU.T

0555.D SCAN508.M Wed Jan 30 09:01:53 2002 Page 13

NYC-WTC_000051547

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NYC-WTC_000051547Source: NYC Law Department, mirrored locally

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