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GCMS results for sample AE00467, Jan 24 2002

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Laboratory report showing GCMS analysis of sample AE00467 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051453–000051470

Folder label: “GCMS X 1/8/02 A 1/11/02

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\MSDCHEM\1\5973N\02JAN11\00467.D Vial: 7 Acq On : 11 Jan 2002 7:05 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 14 10.: 32:38 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 1272086 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 5314219 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2732330 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 4579231 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 4202898 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 3081038 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.7 235 393674 5.44 ug/L 0.00 Spiked Amount 5.000 Recovery = 108.80% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.61 74 9827 0.18 ug/L # 11 20) Dimethylphthalate 18.34 163 438676 2.43 ug/L # 55 21) 2,6-Dinitrotoluene 18.34 165 351356 9.98 ug/L # 17 25) Diethylphthalate 20.00 149 10938 0.06 ug/L 90 3 3) Phenanthrene 22.70 178 6242 0.02 ug/L # 61 3 4) Anthracene 22.70 178 6242 0.03 ug/L # 62 35) Di-n-butylphthalate 24.86 149 109947 0.37 ug/L 96 36) Fluoranthene 26.22 202 11054 0.04 ug/L # 82 3 9) Pyrene 26.85 202 10379 0.03 ug/L 87 40) Butylbenzylphthalate 29.24 149 22721 0.15 ug/L 93 41) Benzo(a)anthracene 30.47 228 53466 0.21 /L 92 42) Bis(2-ethylhexyl)phthalate 31.11 149 49925 0.79 ug /L 78 43) Chrysene 30.56 228 74620 0.30 ug 94 45) Di-n-octylphthalate 32.82 149 23345 0.08 ug/L 92 46) Benzo(b)fluoranthene 33.45 252 31133 0.13 ug/L 89 47) Benzo(k)fluoranthene 33.45 252 31133 0.13 ug/L 89 48) Benzo(a)pyrene 34.25 252 12851 0.06 ug/L 77 49) Indeno(1,2,3-cd)pyrene 37.01 276 9529 0.06 ug/L 82 50) Dibenz(a,h)anthracene 37.10 278 16198 0.11 ug/L 74 51) Benzo(g,h,i)perylene 37.70 276 23831 0.15 ug/L 88

(#) = qualifier out of range (m) = manual integration 00467.D SCAN508.M Mon Jan 14 10:32:39 2002 Page 1

NYC-WTC_000051455

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NYC-WTC_000051455Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.995

machine-extracted · confidence unavailable · Check page ↗

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