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GCMS results for sample AE00471, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00471 with surrogate recovery data on January 18, 2002.

NYC-WTC_000051301–000051317

Folder label: “GCMS X 1/8/02 A 1/10/02

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Scanned page image, NYC-WTC_000051307
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NYC 9/11 Public Portal Document

Llbrary Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\00471.D Vial: 6 Acq On : 10 Jan 2002 6:57 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Butanoic acid, 2-methyl-, m.. Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 4.63 0.16 ug/L 52684 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butanoic acid, 2-methyl-, methyl... 116 C6H1202 000868-57-5 43 2 Butanoic acid, 2-methyl-, methyl... 116 C6H1202 000868-57-5 43 3 Butanoic acid, 2-methyl-, methyl... 116 C6H1202 000868-57-5 43 4 Butanoic acid, 2-methyl-, methyl... 116 C6H12O2 000868-57-5 37 Abundance Scan 110 (4.629 min): 00471 .D (-) m/z 71.10 100.00% 7h 41 57 88

5000

51 101 , MAAmr w 4.20 4.40 4.60 4.80 5.00 01. I .... 1 . ■ ■ i ■ ■ ■ ■ । 1 1 1 1 1 1 11 I 1 1 1 1 1 1 1 m/z 41.10 80.52% /z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #16436: Butanoic acid, 2-methyl-, methyl ester (CAS) $$ Me... 57 88

5000 4-A-4 4.20 4.40> 4.60 4.80 27 101 m/z 57.10 77.70% 33 69

m/z-> 0— ■ ' i ' ’ ■ ■ i ■ ■ ' ' i 1 20 30 40 50 60 . i ' i ' 1 ' ' i ' ' ' ' i ' 70 80 90 100 4 I'............. 110 116120 Abundance #16435: Butanoic acid, 2-methyl-, methyl ester 57 88 II 4.20 4.40 4.60 4.80 5.00 5000 m/ z 88.00 76.07% 101 27 69 | 33 01 TT/D/TTT 'I'" ' 1__________ C ' 1 1 1 1 + I'............. 116 m/z--> 20 30 40 50 60 70 80 90 100 110 120 Abundance #16441: Butanoic acid, 2-methyl-, methyl ester (CAS) $$ Me... .............. , fky 1 ■ । 1 1 ■ 1 । ■ ■ ■ 1 । ■ 1 ' । 1 ■ 88 4.20 4.40 4.60 4.80 5.00 57 m/z 43.10 47.93% 5000 41 29 101 69 0 I | ' 1 r r | I I’ ................. FI’ । । 1 i ' 1 1 .......... 1................... 1 ' 7 । it ’, i [ i f * r। , , ' i ' ' ' ■ I 1 1 1 1 1 1 ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 4.20 4.40 4.60 4.80 5.00

30471.D SCAN508.M Fri Jan 11 10:08:49 2002 Page 3

NYC-WTC_000051307

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NYC-WTC_000051307Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.995

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.995

machine-extracted · confidence unavailable · Check page ↗

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