GCMS analysis results for sample AE00473, Jan 18 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00473 conducted on January 18, 2002.

NYC-WTC_000051283–000051300

Folder label: “GCMS X 1/8/02 A 1/10/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN10\00466.D Vial: 4 Acq On 10 Jan 2002 5:18 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 11 Tetradecanoic acid (CAS) $$... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 27.05 0.15 ug/L 87168 Chrysene-dl2 30.50 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Tetradecanoic acid (CAS) $$ Myri... 228 C14H28O2 000544-63-8 35 2 Dodecanoic acid, silver(l+) salt... 307 C12H24AgO2 018268-45-6 27 3 Tetradecanoic acid (CAS) $$ Myri... 228 C14H2802 000544-63-8 27 4 Tetradecanoic acid (CAS) $$ Myri... 228 C14H2802 000544-63-8 22 Abundance Scan 2074 (27.052 min): 00466.D (-) m/ z 43.05 100.00% 43 57 73

129 5000 www/ Wow 98 111 185 241 26.'80 27.00 27.'20 27.40 oV T’ yyrei rr 1'' i11 m i11 vr TT 1 ■1 ■ ’ 1 m/z 73.00 98.54% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #157233: Tetradecanoic acid (CAS) $$ Myristic acid $$ MYRI... 60 73

5000 r I 1 1 1 r| > ' 129 26.80 27.00 27.20 27.40 27 87 185 228 m/z 57.10 87.72% 171 |

/z-> 01 [ > 20 । > । > 1 40 60 143 ■ । ’ ■ ■ ■ । ■ 4 80 100 120 140 160 180 200 220 240 260 280 300 I " 111 ‘II 1 1 1 1 ■ i' ‘ 1

Abundance #257065: Dodecanoic acid, silver(1 +) salt (CAS) $$ Silver ... 60 73 AA.A.A MA.AA 26.80 27.00 27.20 27.40 183 5000 m/z 60.10 69.71% 129 42 98 157 ... ..... . 307 0' I ' ' ' ' I 1 1 ' I'''' I'''' I''1' I ''' I''' ■ i' 1 ■ ' i ' ' ' • i ' 1 ' ' i ' ' ' ' i 1 '' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #157227: Tetradecanoic acid (CAS) $$ Myristic acid $$ MYRI... 60 73 26.80 27.00 27.20 27.40 m/z 55.00 64.35% 129 5000 87 185 228

m/z-> O-TT 20 40 60 11 I ...... _L 115 143 171

80 100 120 140 160 180 200 220 240 260 280 300 1 1 I 1 1 " I " " T' rr r . > AAMMHIYYYI 26.80 27.00 27.20 27.40

30466.D SCAN508.M Fri Jan 11 10:08:37 2002 Page 13

NYC-WTC_000051299

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NYC-WTC_000051453

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