GCMS blank analysis results for sample AE00327, Jan 2002

NYC 9/11 Public Portal Document

yudit.tdtLOI KCpOLC (NOU Kevewed)

Data File : C:\MSDCHEM\l\5973N\02JAN10\0108B.D Vial: 1 Acq On : 10 Jan 2002 12:21 pm Operator: Sample : lab blank ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 11 10:19:01 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Thu Jan 10 11:01:02 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.71 152 1084204 20.00 ug/L -0.01 10) Naphthalene-d8 13.19 136 4545397 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2358078 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 4022447 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 3648758 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 2630323 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 313869 4.94 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.80%

Target Compounds Qvalue 2) n-Nitroso-dimethylamine 3.60 74 8977 0.19 ug/L # 14 20) Dimethylphthalate 18.34 163 381471 2.45 ug/L # 56 21) 2,6-Dinitrotoluene 18.34 165 299701 9.87 ug/L # 17 35) Di-n-butylphthalate 24.85 149 26577 0.10 ug/L 91 41) Benzo(a)anthracene 30.50 228 8851 0.04 ug/L # 53 42) Bis(2-ethylhexyl )phthalate 31.11 149 233058 1.83 ug/L 94 43) Chrysene 30.50 228 8851 0.04 ug/L # 51 48) Benzo(a)pyrene 34.42 252 9547 0.06 ug/L # 1

(#) = qualifier out of range (m) = manual integration 0108B.D SCAN508.M Fri Jan 11 10:19:02 2002 Page 1

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