GCMS analysis results for sample AE00106, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN25\00106.D Vial: 5 Acq On : 25 Jan 2002 1:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 2 Isothiazole (CAS) $$ 1,2-TH... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 4.24 0.20 ug/L 87635 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Isothiazole (CAS) $$ 1,2-THIAZOLE 85 C3H3NS 000288-16-4 43 2 Thiazole (CAS) $$ 1,3-THIAZOLE 85 C3H3NS 000288-47-1 38 3 Isothiazole 85 C3H3NS 000288-16-4 38 4 Pentane, 2-bromo-4-methyl- 164 C6H13Br 030310-22-6 36 Abundance Scan 76 (4.241 min): 00106. D (-) m/z 85.00 100.00% 41 85 43 5000 60 8789 i M AA/M ■ ■ ’ 1 i ■ ■ 1 ■ i

n/z-> Abundance 30 ...... in 45 50 55 60 65 70 75 80 85 90 95 35 40 5557 I. ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■

#3568: Isothiazole (CAS) $$ 1,2-THIAZOLE i ■ ■ ■ ■ i ’ ■ 3.80 4 00 4.20 4 40 4.60 m/ z 41.10 84.18%

85

A AA , A 1 . , A A 5000 58 3.80 4.00 4.20 4.40 4.60 m/z 43.10 70.29%

m/z-> — dlt 39452 4 87 —PPPT 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #3580: Thiazole (CAS) $$ 1,3-THIAZOLE 85 58 AAIV/ v 1 My 3.80 4.00 4.20 4.40 4.60 5000 m/z 39.10 32.52%

......... . 87 'I......... । I । । i i । । । । । rpn i । . . . . । . ■ | । 1 ■ ■ । • i ■ m/z-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #3569: Isothiazole 85 i

3.80 • ■ ■ ■

4.00 i AL 4.20 4.40 4.60 m/ z 60.10 29.62% 5000 58

39 45 —2- ....... I " "......... I • i • • • ■ i ■ n/z-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.80 4 00 4.20 4.40 4.60

00106.D SCAN508.M Mon Jan 28 09:49:53 2002 Page 4

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