GCMS analysis results for sample AE00165, Feb 2002

NYC 9/11 Public Portal Document LSC Area Percent Report Lata File : C:\MSDCHEM\1\5973N\02FEB04\00165.D Vial: 4 - Acq On 4 Feb 2002 5:37 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.488 7 10 13 rVB 25840 41240 0.26% 0.048% 2 3.602 19 20 25 rBV 29728 52748 0.33% 0.062% 3 4.641 105 111 121 rVB4 10632 41687 0.26% 0.049% 4 5.897 217 221 227 rW 390612 759623 4.70% 0.890% 5 6.000 227 230 243 rVB 53912 150128 0.93% 0.176%

6 9.550 539 541 545 rBV 28083 68732 0.43% 0.080% 7 9.630 545 548 551 rW 29103 67868 0.42% 0.079% 8 9.710 551 555 561 rW 4824661 9543482 59.03% 11.176% 9 9.836 563 566 577 rW 39604 127770 0.79% 0.150% 10 13.192 855 860 865 rBV 6736670 13576071 83.97% 15.899%

11 13.375 873 876 883 rVB 15362 35353 0.22% 0.041% 12 16.549 1149 1154 1159 rW 21596 43200 0.27% 0.051% 13 18.341 1305 1311 1317 rBV 7282611 14980715 92.65% 17.544% 14 22.280 1651 1656 1661 rBV 63265 122673 0.76% 0.144% 15 22.645 1681 1688 1693 rBV2 7079694 16168293 100.00% 18.935%

16 22.771 1697 1699 1713 rVB 91361 249990 1.55% 0.293% 17 27.726 2127 2133 2139 rBV 996810 1763232 10.91% 2.065% 18 30.500 2369 2376 2381 rBV2 6038540 14899385 92.15% 17.449% 19 31.105 2425 2429 2439 rBV 43661 161291 1.00% 0.189% 20 34.416 2713 2719 2759 rBV 4325422 12535917 77.53% 14.681%

Sum of corrected areas: 85389398

•0165.D SCAN508.M Tue Feb 05 09:47:33 2002 Page 1

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