GCMS analysis results for sample AE00110, Feb 2002

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Data File : C:\MSDCHEM\1\5973N\02FEB04\00110.D Vial: 4 . Acq On : 4 Feb 2002 1:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-Propanol, 1- (2-methoxypro. . . Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 9.84 0.38 ug/L 203371 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 83 2 1-Propanol, 2-(2-hydroxypropoxy)... 134 C6H14O3 000106-62-7 56 3 PROPYLENE GLYCOL TRIMER 3 174 C9H1803 000000-00-0 56 4 PROPYLENE GLYCOL TRIMER 1 174 C9H1803 000000-00-0 56 Abundance Scan 566 (9.835 min): 00110.D (-) m/z 59.10 100.00% 50

5000

45 M TTTRrmf

.... W... 4.. 7... 194.......

I 9.40 9.60 9.80 10.00 10.20 0- ■ । • ■ ■ । ■ ■ • ■ । • • ■ ■ ।11 ■ ■ । ■ ■ ■11 • ■ ■ • । ■ • m/z 45.10 13.80% niz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #43942:2-Propanol, 1-(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

5000 ‘1** 9.40 9.60 9.80 10.00 10.20 m/z 73.10 9.79% 31 45 73 104

miz-> 0- 30 40 50 60 4— I......................... T...................130 70 ■ i 1 ■ ■ ■ i ■ ■ ■ ■ i ■ • 1 ■ i ■ 1 ■ ■ i ■ • ' ■ i ■ ■ ■ 1 I 1 ■ 80 90 100 110 120 130 Abundance

5000 #29195:1-Propanol, 2-(2-hydroxypropoxy)- $$ 2-(2-Hydroxyp... 59 MA_ 9.40 m/z 9.60 9.80 10.00 10.20 43.10 9.26% 31 45 103

75 ... I'1 1 ■ i 1 • ’I) • ■ ■i■■ 89 0- i1■■•i ■ ■ ■ ■ i ' 1 ■ ■ i ■ ■ ■ ■ i ■ • ■ 1 l 1 ‘ n/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #78534: PROPYLENE GLYCOL TRIMER 3 59 9.40 . 9.60 . 444 9.80 10.00 10.20 m/ z 42.10 7.99%

5000 41 103

m/z— > O PPPTT ■ ■ll'l . is ■ 30 40 50 60 70 73 87 ■ i ■ ■ ■'' i ■ ■ ■ ■ i'1 1 ■ ' i ■ ■

80 90 100 110 117 120 130 i ' 1 ■ 1 I ■ ‘ 130 AN, M. 9.40 9.60 9.80 10.00 10.20

0110.D SCAN508.M Tue Feb 05 09:47:02 2002 Page 11

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