GCMS blank analysis results for sample AE00110, Feb 2002

NYC 9/11 Public Portal Document ~pul ASpOL L

Data File : C:\MSDCHEM\l\5973N\02FEB04\0204BB.D Vial: 1 Acq On : 4 Feb 2002 10:58 am Operator: Sample : lab blank l/4b Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\ SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 10 5,6 - INDOLEDIOL Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 20.00 0.07 ug/L 47502 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW Mol Form . CAS# Qual 1 5,6-INDOLEDIOL 149 C8H7NO2 000000-00-0 53 2 1,2-Benzenedicarboxylic acid, mo... 222 C12H1404 000131-70-4 50 (0 3 Benzoic acid, 2-(1-oxopropyl)- 178 C10H10O3 002360-45-4 45 V (/* 4 Phthalic acid, 2-hexyl ester 250 C14H1804 000000-00-0 39 W Abundance Scan 1456 (19.997 min): 0204BB.D (-) m/z 149.00 100.00% 149

5000

44 65 76 104 177 .M 19.60 19.80 20.00 20.20 20.40 0 ..... 1.11,.. ■ i ' * ■ ■ i ■ ■ m/z 177.00 28.23% ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #45075:5,6-INDOLEDIOL 149

5000 103 19.60 19.80 20.00 20.20 20.40 m/z 65.10 16.18% 50 65 76 92 120 27 ... • 1 i ■ 1 ■ 1 i ■ ■ ■ ■ I ‘ 1 ■ • i ■ • ■ ■ i 1 • 0 I 11 1 I 1 n/z—> 20 40 60 80 100 120 140 160 180 200 220 Abundance #147072:1,2-Benzenedicarboxylic acid, monobutyl ester 149

19.60 19.80 20.00 20.20 20.40 5000 m/z 150.00 13.90% 56 I 76 12293 105 167 mfc-> 0-1— । 20 40 160 80 7 100 120 140 L 160 III. 222 ‘ 1 । » । । < i < । । i । i ryri-i i । i i i i j i i 180 200 220 Abundance #83206: Benzoic acid, 2-(1-oxopropyl)- 149 19.60 19.80 20.00 20.20 20.40 m/z 176.10 13.47% 5000

27 50 65 76 93 104 121 .. | I 0 i 1 ‘ ■ i ■ ■ ■ ■ i 1 — TTt ' iI ■ ■133 ■' • i ■ ■ 160 n/z—> 20 40 60 80 100 120 140 160 180 200 220 19.60 19.80 20.00 20.20 20.40

204BB.D SCAN508.M Tue Feb 05 09:47:47 2002 Page 12

NYC-WTC_000050641