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GCMS analysis results for sample AE00100, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050354–000050369

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN23\00100.D Vial: 3 Acq On : 23 Jan 2002 4:36 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Toluene Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

4.37 0.23 ug/L 83755 1,4-Diehlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Toluene 92 C7H8 000108-88-3 90 2 Toluene $$ Benzene, methyl $$ Me... 92 C7H8 000108-88-3 87 3 Toluene 92 C7H8 000108-88-3 87 4 Benzene, methyl- (CAS) $$ Toluen... 92 C7H8 000108-88-3 87 Abundance Scan 87 (4.367 min): 00100.D (-) m/z 91.10 100.00% 91

5000

39 43 51 85 65 4.00 4.20 4.40 4.60 4.80 01 m -HH —poope m/z 92.10 60.07% Tl/Z-> 3035404550556065 70 7580 85 90 95 100 Abundance #5542: Toluene 91

5000 -------------------- 4.00 4.20 4.40 4.60 4.80 m/z 65.00 10.15% E 51 65 45 • 1 01 1I1111I1 ■ III1I ■ I I11 ■ 11111I111II ■ 1111111III1 ■ r a I rr 1111111111111I ‘ i “ " i'1 miz—> 303540 45 50556065 70 75 808590 95 100 Abundance #5543: Toluene $$ Benzene, methyl $$ Methacide $$ Methylbe... 91 nnnn/m—m—dm/nnB7 4.00 4.20 4.40 4.60 4.80 5000- m/z 39.10 8.82%

39 45 51 65 Of nPmmmmmaRmmmmm 1 ‘ 14'1111 ■ miz-> Abundance 303540 45 50556065 70 75 808590 #5541: Toluene 91 95 100 AA 4.00 4.20 • • l ' " ■ • J • • ■ • I • 4.40 4.60 4.80 m/z 63.10 7.07% 5000

51 65 37 0 ■' 11 ■ • ■ i ■ ‘ ■ i ■ “ ‘ i ■ — TH +pope 1 1 I 1 1 1 1 1 1 ' V) ... > or I I I ' /z—> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 4.00 4.20 4.40 4.60 4.80

00100.D SCAN508.M Thu Jan 24 09:57:09 2002 Page 4

NYC-WTC_000050361

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NYC-WTC_000050361Source: NYC Law Department, mirrored locally

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