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GCMS analysis results for sample AD31645, Jan 25 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050222–000050239

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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Scanned page image, NYC-WTC_000050229
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NYC 9/11 Public Portal Document

Library Search Compound Report Data .File : C:\MSDCHEM\1\5973N\O2JAN22\31645 .D Vial: 1 Acq On : 22 Jan 2002 12:12 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Toluene Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 4.37 0.25 ug/L 77098 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Toluene 92 C7H8 000108-88-3 90 2 Toluene 92 C7H8 000108-88-3 90 3 Benzene, methyl- (CAS) $$ Toluen... 92 C7H8 000108-88-3 90 4 Toluene $$ Benzene, methyl $$ Me... 92 C7H8 000108-88-3 90 Abundance Scan 87 (4.367 min): 31645.D (-) m/z 91.10 100.00% S1

5000

4.00 4.20 4.40 4.60 4.80 mlz-> ....225 .......1,117011170101784* 30354045505560657075808590 95 100 । ■ ।1 ■1 ■ । ‘ ■ m/z 92.10 64.49% Abundance #5542: Toluene 91

5000 4.00' 4.20 4.40 4.60 4.80 m/z 65.10 12.23% 45 51 65 14-1 ■ ■ ' | I ' I | | i I ■ I | I I I | | | 1 | | | i nri I rr n I I | l 1 I I | ■ ■ 11 ■ > 11 ‘ * niz—> 30 35 40 4550556065 70 75 808590 95 100 Abundance #5541: Toluene SI

4.00 4.20 4.40 4.60 4.80 5000 m/z 51.00 8.44%

51 65 37 3 61,| | • • l * ‘ ■ ■ } * > • • t ■ ■ ■ ‘ I * ‘ I' i " 111'' • 11 ATITT11 | t 11 ! | | । i i । i ri । । i i i i । i i i i । i i i I ] I m/z—> 30 35 404550556065 70 75808590 95 100 Abundance #5539: Benzene, methyl- (CAS) $$ Toluene $$ CP 25 $$ Methy... SI 4.00 4.20 4.40 4.60 4.80 m/z 39.10 8.12% 5000

. F4 65 45 51 61 1 M—mmmmnammmmm Pmmmm ' ‘ i • ‘ ‘ i ‘ ■ 1 ■ i ' ' ' ' i 1 ‘ ‘ 1 i' m/z—> 3035404550556065 70 75808590 95 100 4.00 4,20 4.40 4.60 4.80

31645.D SCAN508.M Thu Jan 24 13:50:34 2002 Page 4

NYC-WTC_000050229

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NYC-WTC_000050229Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

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