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GCMS blank analysis for sample AE00005, Feb 8 2002

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Blank analysis report for GCMS testing of sample AE00005 showing non-detectable levels of target compounds.

NYC-WTC_000050079–000050087

Folder label: “GCMS X 1/3/02 A 1/24/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN2402\LB.D Vial: 3 Acq On : 24 Jan 2002 2:01 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 8 9:18 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 2) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.76 178 763 N.D. 3 4) Anthracene 24.76 178 763 N.D. 35) Di-n-butylphthalate 26.78 149 2362 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 32.78 228 3983 N.D. 42) Bis(2-ethylhexyl)phthalate 33.09 149 4278 N.D. 43) Chrysene 32.87 228 679 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 35.82 252 257 N.D. 47) Benzo(k)fluoranthene 35.90 252 479 N.D. 4 8) Benzo(a)pyrene 36.84 252 4067 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration LB.D GCMS0103.M Fri Feb 08 09:18:42 2002 Page 2

NYC-WTC_000050081

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NYC-WTC_000050081Source: NYC Law Department, mirrored locally

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GCMS blank analysis report, Feb 2002 · Box DEP Box 12

NYC-WTC_000005159

Blank sample analysis report confirming no contamination above method detection limits for target compounds analyzed on February 1, 2002.

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