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GCMS blank analysis, sample AD31432, Jan 2002

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Blank analysis report for DEP sample AD31432 showing non-detect levels for volatile organic compounds from January 22, 2002.

NYC-WTC_000016555–000016563

Folder label: “GCMS X 12/31/01 A 1/18/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JANI802\LB.D Vial: 4 Acq On : 18 Jan 2002 6:34 pm Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 15:01 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.78 178 1333 N.D. 34) Anthracene 24.78 178 1333 N.D. 35) Di-n-butylphthalate 26.80 149 82433 0.54 ug/1 96 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.29 149 941 N.D. 41) Benzo(a)anthracene 32.87 228 3595 N.D. 42) Bis(2-ethylhexyl)phthalate 33.10 149 8276 N.D. 43) Chrysene 32.87 228 3595 N.D. 45) Di-n-Octylphthalate 34.85 149 1678 N.D. 46) Benzo(b)fluoranthene 35.85 252 1885 N.D. 47) Benzo(k)fluoranthene 35.91 252 6937 N.D. 48) Benzo(a)pyrene 36.71 252 1638 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 41.54 276 413 N.D.

(#) = qualifier out of range (m) = manual integration LB.D GCMS0103.M Wed Feb 06 15:01:59 2002 Page 2

NYC-WTC_000016557

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NYC-WTC_000016557Source: NYC Law Department, mirrored locally

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GCMS blank analysis report, Feb 2002 · Box DEP Box 12

NYC-WTC_000005159

Blank sample analysis report confirming no contamination above method detection limits for target compounds analyzed on February 1, 2002.

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