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← Document results/DEP Box 28/GCMS X 1/2/02 A 1/3 - 1/4/02
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GCMS analysis results for sample AD29292, Jan 22 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AD29292 including unknown compounds and surrogate recovery data.

NYC-WTC_000049823–000049832

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\JAN0302\29292.D Vial: 23 Acq On 4 Jan 2002 7:58 am Operator: 209 GALOS Sample gems scan 1/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.60 0.57 ug/1 111315 1,4-Dichlorobenzene-d4 11.52 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2 - Propanone ,zl, 1,1-trichloro- 160 C3H3C130 000918-00-3 50 2 Ethanol, 2,2,2-trichloro- 148 C2H3C130 000115-20-8 9 3 2-Acetyl-1, 4,5,6-tetrahydropyridine 125 C7H11NO 000000-00-0 7 4 2-Buten -amine, N-butyl-, (Z) - 127 C8H17N 062337-87-5 7 Abundance ( Scan 279 (7.605 min): 29292.D (-) m/ z 43.00 100.00% I 43

5000

I • • • 1 i TTIBBGnmnnm . 125 35 . at 53ltimhonajhega 144/* 63 72 82 97 n 117 11 7.20 7.40 7.60 7.80 8.00 • • | ' t i i-q .... । * i ’ I i j'j'j 1**’’I’’*1111 m/z 124.85 12.84% miz-? 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #12247:2-Propanone, 1,1,1-trichloro- 48

5000 7.20 7.40 7.80 7.80 8.00 15 m/z 81.95 10.82% 35 85 97 117 125 I ! . • It • • ’’7111111121115171993B303"3"B’B33531 ■ |T-> I I | I ll l"| 1 i ■ • • 11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66531: Ethanol, 2,2,2-trichloro- 31 i ■ • • • i • 1 1 1 i 1 1 I 1 ' 1 1 I ' 1 7.20 7.40 7.60 7.80 8.00 5000 49 m/z 127.0.0 10.48% 77 113 61 84 ! । 150 1111 ■ • ■ 11 ■ • ‘ i1''11 • • • • i •11111'111111111 *111111 miz-> 10 2030405060 70 8090 100 110 120 130 140 150 Abundance #4332:2-Acetyl-1,4,5,6-tetrahydropyridine । । i i । । i । 1 T | I J' I I T I ) 43 7.20 7.40 7.60 7.80 8.00 54 82 m/z 35.00 8.88% 5000 125

* ‘I**‘ 'I ‘‘ H »* * st ‘ ‘ ‘ ‘ । • 1 • i • ■ •11 ■' ■1 “I ' Y ■“noI l' I'l ■ I I ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 7.20 7.60 ' 7.80 “ 8.00

29292.D GCMS0103.M Fri Jan 11 08:30:33 2002 Page 2

NYC-WTC_000049831

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NYC-WTC_000049831Source: NYC Law Department, mirrored locally

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