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GCMS results for sample AE08930, April 26, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08930 conducted on April 26, 2002.

NYC-WTC_000049341–000049349

Folder label: “GCMS X 4/15/02 A 4/24/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report ' Data File : C:\HPCHEM\1\DATA\APR2302\8930.D Vial: 10 Acq On : 23 Apr 2002 11:13 pm Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 8.182 339 342 370 rVB 311509 870139 21.63% 4.249% 2 12.212 775 781 797 rVB 1114224 2751956 68.41% 13.437% 3 14.810 1058 1064 1071 rBV 47941 88790 2.21% 0.434% 4 15.839 1170 1176 1193 rBV 1669789 3525331 87.64% 17.213% 5 21.145 1748 1754 1768 rBV 1989699 4022527 100.00% 19.641% 6 23.284 1979 1987 1993 rBV 177985 346205 8.61% 1.690% 7 25.588 2231 2238 2249 rBV2 1866584 3853938 95.81% 18.818% 8 33.639 3108 3115 3135 rBV2 1231218 2882730 71.66% 14.076% 9 37.871 3567 3576 3595 rBV2 720849 2138840 53.17% 10.443%

Sum of corrected areas: 20480456 8930.D GCMS0412.M Wed Apr 24 08:37:46 2002

NYC-WTC_000049345

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NYC-WTC_000049345Source: NYC Law Department, mirrored locally

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