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GCMS analysis results for sample AE08937, April 29 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08937 conducted on April 29, 2002, showing surrogate recovery.

NYC-WTC_000049213–000049223

Folder label: “GCMS X 4/15/02 A 4/22/02

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Scanned page image, NYC-WTC_000049220
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\042202\8937.D Vial: 10 Acq On : 22 Apr 2002 6:32 pm Operator: Bohlk Sample : SAMPLE 8937 4/15/02, FB Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L Peak Number 1 Benzene, methyl- (CAS) $$ T... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 3.87 8.55 ug/L 526808 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, methyl- (CAS) $$ Toluen... 92 C7H8 000108-88-3 94 2 Toluene $$ Benzene, methyl $$ Me... 92 C7H8 000108-88-3 91 3 Toluene 92 C7H8 000108-88-3 91 4 1,3,5-Cycloheptatriene (CAS) $$ — 92 C7H8 000544-25-2 91 Abundance Scan 135 (3.872 mln): 8937.D (-) m/z 91.10 100.00% 91

5000

■ ■ ■ • i • ■ ■ ■ i' ■ • ■ i • • ■ •T1 • • ■

0- -558 39 . 51 65 86 m/z 3.60 3.80 4.00 4.20 92.10 60.33% 111 '"’‘r1 ■ • i ■ miz-> 20 30 40 50 60 70 80 90 100 Abundance #5539: Benzene, methyl- (CAS) 5$ Toluene $$ CP 25 $$ Methy... 91

5000 Irmorptosstroormomo 3.60 3.80 4.00 4.20 m/z 65.10 14.34%

28 3945/51 6Q |? 77 86 , 0- • ‘ i ■ • ‘ 1 i 1 ■ • । | ' >,l ■ | । • • .p'l'i . । , rn । . > i , | । 1 n/z-> 20 30 40 50 60 70 80 90 100 Abundance #5543: Toluene $$ Benzene, methyl $$ Methacide $$ Methylbe... 91

■ ■ i ■ ‘ 3.60 3.80 4.00 4.20 5000 m/z 51.10 8.29%

miz-> .... 27 39 45 51 eo,55 77 86, 0 1 1 1 1 1 1 1 1' 1 i l'l'i i'l rjJf> i i fl'l'i r । i > i > । i > i-i’I'I 20 30 40 50 60 70 80 90 100 Abundance #5541: Toluene panMokton 91 T T T T 3.60 3.80 4.00 4.20 m/z63.10 7.87%

5000

39 *51 65 n/z—> 127 0- —1—** -n-r-j-r 20 30 .1 45 T|. 57 .,1.1. 40 50 60 70 77 80 86,. 90 100 • • i1 ■ ■11 3.60 3.80 4.00 4.20 4 8937.D 5080402BBC.M Thu Apr 25 14:37:09 2002 Page 3

NYC-WTC_000049220

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NYC-WTC_000049220Source: NYC Law Department, mirrored locally

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