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GCMS analysis results for sample AE08762, April 25, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08762 conducted on April 25, 2002, showing detection of unknown compounds.

NYC-WTC_000049124–000049133

Folder label: “GCMS X 4/12/02 A 4/23/02

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Scanned page image, NYC-WTC_000049129
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C: \HPCHEM\ 1 \DATA\APR2 202\8762.D Vial: 24 Acq On : 23 Apr 2002 7:33 am Operator: Sample : gc/ms scan 4/12 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.184 339 342 373 rVB 349194 887096 22.25% 4.376% 2 12.214 775 781 797 rBV 1142360 2717733 68.15% 13.406% 3 14.812 1059 1064 1069 rVB 40281 75093 1.88% 0.370% 4 15.840 1170 1176 1193 rBV 1666669 3511117 88.05% 17.320% 5 21.146 1748 1754 1766 rBV 1995623 3987755 100.00% 19.671% 6 23.285 1980 1987 1994 rBV 191113 374539 9.39% 1.848% 7 25.590 2231 2238 2249 rBV2 1845808 3829902 96.04% 18.893% 8 33.641 3108 3115 3134 rBV2 1238524 2840397 71.23% 14.011% 9 37.873 3567 3576 3593 rBV2 687655 2048368 51.37% 10.104%

Sum of corrected areas: 20272000 8762.D GCMS0412.M Tue Apr 23 14:24:07 2002

NYC-WTC_000049129

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NYC-WTC_000049129Source: NYC Law Department, mirrored locally

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