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GCMS analysis results for sample AE08685, April 26, 2002

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GCMS laboratory report for sample AE08685 analyzed on April 26, 2002, by analyst DLV.

NYC-WTC_000048912–000048922

Folder label: “GCMS X 4/11/02 A 4/22/02

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NYC 9/11 Public Portal Document

* Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR2202\8685.D Vial: 7 Acq On : 22 Apr 2002 3:02 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Nonadecanol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 8.25 1.41 ug/1 177924 1,4-Dichlorobenzene-d4 12.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Nonadecanol 284 C19H40O 052783-43-4 9 2 1-Eic anol 298 C20H42O 000629-96-9 9 3 Ethan 1, 2,2,2-trichloro- 148 C2H3C130 000115-20-8 9 4 Decane, 1-fluoro- 160 C10H21F 000334-56-5 9 Abundance Scan 349 (8.252 min): 8685. D(-) m/z 43.00 100.00% 43

5000

125 1 ■ i ' 1 ■ I' ■ ■ 61 83 97 8.00 8.20 8.40 8.60

m/z—> t’’ 20 40 4. . 60 80 100 120 ii 140 160 180 200 220 240 260 280 m/z 124.80 17.59% Abundance #40237: Nonadecanol 43 57

5000 83 31 71 8.00 8.20 8.40 8.60 97 m/z 96.90 11.90% ,i 111 Il I M 125 252 266 i ■ ■ ■ • i •' ■ ■ i1 ■'11•11■।• i ■ ■ • • i' ■ ■ ■ i ■ ■ ■ •i•■•■i‘‘' 11 ■ ■ 1 • i ■ ■ •11 1 1 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #42525: 1-Eicosanol 43 57 8.00 8.20 8.40 8.60 5000 83 m/z 48.90 10.37% 71

mz—> 20 27

। ■ ■i ■ i‘ ■ 40 ‘13 1-r-p 60 80 97

'I1! 111 125.252, . . 280 "MMMaAlupary/ 100 120 140 160 180 200 220 240 260 280 Abundance #66531: Ethanol, 2,2,2-trichloro- 31 8.00 8.20 8.40 8.60 m/z 82.95 10.31%

5000 49 77 113

m/z—> 1’3 20 40 UO4 60 80 150 100 120 140 160 180 200 220 240 260 280 8.00 8.20 8.40 8.60

NYC-WTC_000048920

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NYC-WTC_000048920Source: NYC Law Department, mirrored locally

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