GCMS analysis results for sample AE08685, April 26, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR2202\8685.D Vial: 7 Acq On : 22 Apr 2002 3:02 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 4-Tetradecanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.17 0.59 ug/1 88132 Chrysene-dl2 33.64

Hit# of 5 Tentative ID . MW MolForm CAS# Qual 1 4-Tetradecanol 214 C14H30O 001653-33-4 72 2 1-Octadecanol 270 C18H380 000112-92-5 72 3 l-Heptadecanol 256 C17H360 001454-85-9 72 4 1-Octadecene 252 C18H36 000112-88-9 58 Abundance Scan 2845 (31.166 min): 8685.D (-) m/z 55.00 100.00% 55

43 5000 83 97 69 — —"*9*11—4 111 127 II .li, I il 141 153 30.80 31.00 31.20 31.40 207 — T [1 1 I Th J 14 J 1 . iI ‘ ‘*I*‘‘I‘* m/z 43.05 54.33% miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #26420:4-Tetradecanol 43 57 83 97 A A A 4 1 , I.YTMA AM A 5000 70 30.80 31.00 31.20 31.40 111 125 m/Z 83.05 45.58%

T.T 111/8 I I 166 196 miz-> 40 60 80 100 “ 120 ' 140 ' 160 -180 ‘ 200 ' 220 ‘ ‘ 240 ' Abundance #72029:1-Octadecanol 43 55 69 83 97 30.80 31.00 31.20 31.40 5000 m/z 57.00 44.38% 111

miz-> Abundance * * I* ' 40 60 1 • i1 80 100 L 125 224 252 • ' i ■ ■ ■ • I ■ ■ ■ ■ i ■ ■ • ‘ I ■ ■ ■ ‘ i 1 • ■ ■ i ■ • ‘ ‘ i 120 140 160 180 #35210:1-Heptadecanol 200 220 240 55 69 93 83 3080 31.00 31.20 31.40 m/z 73.00 43.74% 97 5000- 111

m/z—> • 1 i ’ ‘ 40 1nB 60 ■ ‘ 1 80 125

180 210 238 i • • ' * i ■ • ‘ * i • • 1 ‘ i 1 1 ' ■ i ' * * * i * • ’ * i ■ ■ ■ • i ‘ 1 100 120 140 160 200 220 240 — A 1 30.80 31.00 31.20 31.40 __ A T-p-

NYC-WTC_000048921