GCMS analysis results for sample AE08685, April 26, 2002

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GCMS laboratory report for sample AE08685 analyzed on April 26, 2002, by analyst DLV.

NYC-WTC_000048912–000048922

Folder label: “GCMS X 4/11/02 A 4/22/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR2202\8685.D Vial: 7 Acq On : 22 Apr 2002 3:02 pm Operator : Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 23 7:53 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.21 152 472085 20.00 ug/1 -0.03 10) Naphthalene-d8 15.84 136 1724792 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 978250 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.58 188 1463750 20.00 ug/1 -0.03 39) Chrysene-dl2 33.64 240 1051667 20.00 ug/1 -0.03 45) Perylene-dl2 37.88 264 742960 20.00 ug/1 -0.04 System Monitoring Compounds 28) TCMX 23.29 209 47777 9.74 ug/L -0.04 Spiked Amount 10.000 Recovery = 97.40% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.91 128 207 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. \ 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.55 165 184 N.D. 25) Diethylphthalate 22.63 149 490 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. (#) = qualifier out of range (m) = manual integration OCOL no M Pse Amv m . EA . a C onno Dace 1 NYC-WTC_000048914

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NYC-WTC_000048914Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE08686, April 26, 2002 · Box DEP Box 27

NYC-WTC_000048923

GCMS laboratory report for sample AE08686 analyzed on April 26, 2002, by analyst DLV.

1 shared topics · Same agency, volume and box · similarity 0.998