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GCMS analysis results for sample AE08681, April 23, 2002

Machine-extracted title · confidence 100%

GCMS laboratory report for sample AE08681 analyzed on April 23, 2002, by analyst DLV.

NYC-WTC_000048846–000048856

Folder label: “GCMS X 4/11/02 A 4/15/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report * Data File : C:\HPCHEM\1\DATA\APR1202\8681.D Vial: 13 Acq On : 15 Apr 2002 7:50 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title . : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.379 141 145 160 rBV 170325 417295 9.95% 1.950% 2 8.206 340 344 369 rBV 333682 859703 20.49% 4.017% 3 12.227 777 782 800 rBV 1115373 2776985 66.19% 12.974% 4 14.834 1061 1066 1073 rVB 34397 69612 1.66% 0.325% 5 15.862 1172 1178 1196 rBV 1700676 3602413 85.86% 16.831% 6 21.168 1750 1756 1771 rBV 2053942 4195525 100.00% 19.602% 7 23.308 1981 1989 1994 rBV 197527 389738 9.29% 1.821% 8 25.612 2233 2240 2252 rBV 1915896 4017616 95.76% 18.771% 9 33.663 3110 3117 3135 rBV2 1220398 2876480 68.56% 13.439% 10 37.904 3570 3579 3596 rBV2 725563 2198436 52.40% 10.271%

Sum of corrected areas: 21403803 8681.D GCMS0412.M Tue Apr 16 15:42:15 2002

NYC-WTC_000048851

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NYC-WTC_000048851Source: NYC Law Department, mirrored locally

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