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GCMS surrogate recovery data for sample AE07765, April 2002

Machine-extracted title · confidence 100%

Record of surrogate compound recovery rates for sample AE07638 analyzed on April 18, 2002.

NYC-WTC_000040269–000040278

Folder label: “GCMS X 4/3/02 A 4/10/02

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Scanned page image, NYC-WTC_000040274
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\APR1102\7765.D Vial: 14 Acq On : 12 Apr 2002 3:10 am Operator: Sample : gc/ms scan 4/3 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.227 776 782 797 rBV 867914 2106722 68.81% 14.402% 2 14.826 1060 1065 1072 rVB 78000 148610 4.85% 1.016% 3 15.863 1172 1178 1193 rBV 1270949 2676616 87.42% 18.298% 4 21.169 1749 1756 1770 rBV 1494999 3061816 100.00% 20.931% 5 23.308 1980 1989 1994 rBV 132809 269723 8.81% 1.844%

6 25.603 2233 2239 2249 rBV2 1322786 2902928 94.81% 19.845% 7 25.750 2252 2255 2264 rVB 11283 30680 1.00% 0.210% 8 27.577 2448 2454 2460 rBV 34218 64291 2.10% 0.440% 9 33.663 3110 3117 3130 rBV2 848304 1932183 63.11% 13.209% 10 37.896 3570 3578 3604 rBV2 473844 1434319 46.85% 9.805%

Sum of corrected areas: 14627888

7765.D GCMS0412.M Fri Apr 12 09:28:00 2002

NYC-WTC_000040274

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NYC-WTC_000040274Source: NYC Law Department, mirrored locally

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