GCMS analysis results for sample AE06427, April 23, 2002

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GCMS laboratory report for sample AE06427 analyzed on April 23, 2002, by analyst DLV.

NYC-WTC_000048810–000048826

Folder label: “GCMS X 4/11/02 A 4/15/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APR0405\6427.D Vial: 13 Acq On 6 Apr 2002 1:49 am Operator : Sample gc/ms scan 3/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 10 12:18 2002 Quant Results File: GCMS0408.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 10 10:43:06 2002 • Response via : Initial Calibration DataAcq Meth : GCMS0403 W

Internal Standards R.T. Qlon Response Cone Units Dev (Min). 1) 1,4-Dichlorobenzene-d4 12.24 152 496644 20.00 ug/1 -0.02 10) Naphthalene-d8 15.89 136 1802589 20.00 ug/1 -0.02 I7) Acenaphthene-dl0 21.19 164 1013816 20.00 ug/1 -0.01 3 0) Phenanthrene-dl0 25.63 188 1416040 20.00 ug/1 -0.02 39) Chrysene-dl2 33.69 240 696727 20.00 ug/1 -0.03 45) Perylene-dl2 37.93 264 386228 20.00 ug/1 -0.02 System Monitoring Compounds 28) TCMX 0.00 209 0 0.00 ug/mL Spiked Amount 4.000 Recovery = 0.00% 38) 2,4-DDD 30.70 235 63768 4-.89 ug/mL 0.20 Spiked Amount 5.000 Recovery 2.3° 97-8056362 0 Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachioroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.67 149 768 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 9) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. (#) = qualifier out of range (m) = manual integration 6427.D GCMS0408.M Wed Apr 10 12:19:01 2002 Page 1

NYC-WTC_000048820

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GCMS analysis results for sample AE06424, April 23, 2002 · Box DEP Box 27

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GCMS laboratory report for sample AE06424 analyzed on April 23, 2002, by analyst DLV.

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