GCMS surrogate recovery data for sample AE06428, April 2002

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Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR0405\6428.D Vial: 14 Acq On 6 Apr 2002 2:48 am Operator: Sample gc/ms scan 3/19 Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 10 12:19 2002 Quant Results File: GCMS0408.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 10 10:43:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 446884 20.00 ug/1 -0.01 10) Naphthalene-d8 15.89 136 1628481 20.00 ug/1 -0.02 17) Acenaphthene-diO 21.19 164 918787 20.00 ug/1 -0.01 30) Phenanthrene-diO 25.63 188 1277304 20.00 ug/1 -0.02 39) Chrysene-dl2 33.69 240 604558 20.00 ug/1 -0.03 45) Perylene-dl2 37.93 264 327537 20.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 0.00 209 0 0.00 ug/mL Spiked Amount 4.000 Recovery = 0.00% 38) 2,4-DDD 30.70 235 68360 5.81 ug/mL 0.20 Spiked Amount 5.000 Recovery = 116.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.47 74 196 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21 -oxybis(l-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.67 149 616 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D.

(#) = qualifier out of range (m) = manual integration 6428.D GCMS0408.M Wed Apr 10 12:20:21 2002 Page 1

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