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GCMS analysis results for sample AE06413, April 23, 2002

Machine-extracted title · confidence 100%

GCMS laboratory report for sample AE06413 analyzed on April 23, 2002, by analyst DLV.

NYC-WTC_000048758–000048775

Folder label: “GCMS X 4/11/02 A 4/15/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report ' Data File C: \HPCHEM\ 1 \DATA\APR04 05\ 6413 . D Vial: 8 Acq On 5 Apr 2002 6:54 pm Operator: Sample gc/ms scan 3/19 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 12.246 778 784 802 rBV 949138 2410690 69.17% 15.720% 2 14.844 1062 1067 1072 rVB 45497 84419 2.42% 0.550% 3 15.881 1174 1180 1198 rBV 1473596 3071978 88.14% 20.032% 4 21.188 1752 1758 1776 rBV 1689342 3485290 100.00% 22.728% 5 25.631 2235 2242 2254 rBV2 1465234 3173935 91.07% 20.697% 6 30.708 2790 2795 2801 rBV 161221 314133 9.01% 2.048% 7 33.691 3113 3120 3139 rBV 722160 1674173 48.04% 10.917% 8 33.912 3139 3144 3153 rVB 30522 73680 2.11% 0.480% 9 37.933 3574 3582 3602 rBV2 342575 1046714 30.03% 6.826%

Sum of corrected areas: 15335012 6413.D GCMS0408.M Wed Apr 10 12:22:51 2002

NYC-WTC_000048772

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NYC-WTC_000048772Source: NYC Law Department, mirrored locally

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