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GCMS analysis results for sample AE08486, May 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE08486 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000048647–000048659

Folder label: “GCMS X 4/10/02 A 4/20/02

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Scanned page image, NYC-WTC_000048649
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\020419\08484.D Vial: 21 Acq On : 20 Apr 2002 3:49 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 26 15:15:22 2002 Quant Results File: SCAN020418.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Mon Apr 22 08:00:39 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Diehlorobenzene-d4 11.38 152 11756322 40.00 ug/1 -0.05 10) Naphthalene-d8 16.53 136 45164665 40.00 ug/1 -0.07 17) Acenaphthene-dl0 24.46 164 24837976 40.00 ug/1 -0.06 30) Phenanthrene-diO 31.72 188 37419269 40.00 ug/1 -0.06 38) Chrysene-dl2 39.94 240 29125821 40.00 ug/1 -0.07 44) Perylene-dl2 43.16 264 21454469 40.00 ug/1 -0.04

System Monitoring Compounds 27) TCMX 27.54 207 1145820 7.43 ug/1 -0.07 Spiked Amount 10.000 Recovery = 74.30% Target Compounds Qvalue 35) Di-n-butylphthalate 34.81 149 100395 0.08 ug/1 96 43) Bis(2-ethylhexyl)phthalate 40.53 149 57371 0.08 ug/1 94

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08484.D SCAN020418.M Fri Apr 26 15:16:27 2002 Page 1

NYC-WTC_000048649

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NYC-WTC_000048649Source: NYC Law Department, mirrored locally

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