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GCMS calibration table and instrument parameters, Apr 2002

Machine-extracted title · confidence 90%

Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.

NYC-WTC_000048583–000048597

Folder label: “GCMS X 4/10/02 A 4/15/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR1202\8481.D Vial: 26 Acq On : 16 Apr 2002 9:08 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 17 9:44 2002 iQuant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Apr 16 14:55:12 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.62 178 486 N.D. 35) Anthracene 25.62 178 486 N.D. 36) Di-n-butylphthalate 27.58 149 2895 N.D. 37) Fluoranthene 0.00 202 0 N.D. 4 0) Pyrene 0.00 202 0 N.D. 41) Butylbenzylphthalate 0.00 149 0 N.D. 42) Benzo(a)anthracene 33.67 228 2293 N.D. 43) Bis(2-ethylhexyl)phthalate 33.88 149 3537 N.D. 44) Chrysene 33.67 228 2293 N.D. 46) Di-n-Octylphthalate 0.00 149 0 N.D. 47) Benzo(b)fluoranthene 0.00 252 0 N.D. 48) Benzo(k)fluoranthene 0.00 252 0 N.D. 49) Benzo(a)pyrene 37.91 252 2845 N.D. 50) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 8481.D GCMS0412.M Wed Apr 17 09:45:18 2002 Page 2

NYC-WTC_000048584

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NYC-WTC_000048584Source: NYC Law Department, mirrored locally

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