GCMS analysis results, Sample AE05750, April 18, 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C : \HPCHEM\ 1 \DATA\APR12025750.D Vial: 19 Acq On : 16 Apr 2002 1:43 am Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.206 340 344 371 rVB 314288 819710 19.93% 4.066% 2 12.227 777 782 799 rBV 1125294 2778674 67.57% 13.782% 3 14.825 1060 1065 1070 rBV 29679 59003 1.43% 0.293% 4 15.863 1172 1178 1196 rBV 1669977 3598579 87.50% 17.849% 5 21.059 1739 1744 1749 rBV 23092 46333 1.13% 0.230%

6 21.169 1749 1756 1769 rBV 2031959 4112450 100.00% 20.397% 7 23.308 1982 1989 1997 rBV 206876 409309 9.95% 2.030% 8 25.612 2233 2240 2252 rBV2 1743671 3762693 91.50% 18.663% 9 25.750 2252 2255 2272 rVB2 15777 49939 1.21% 0.248% 10 33.663 3110 3117 3137 rBV2 1080565 2558969 62.22% 12.692%

11 37.905 3570 3579 3601 rBV 626506 1966093 47.81% 9.752%

Sum of corrected areas: 20161752

5750.D GCMS0412.M Wed Apr 17 09:46:54 2002

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